15548-56-8Relevant articles and documents
Preparation method of cyclopentene triketone
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Paragraph 0020; 0021; 0022; 0023; 0024; 0025; 0026-0030, (2017/08/29)
The invention discloses a preparation method of cyclopentene triketone, and belongs to the technical field of battery electrolyte additives. The method comprises the steps of adopting cyclopentene as a raw material, carrying out bromination reaction with NBS in an organic solvent in the presence of a catalyst, heating until refluxing during reaction, controlling the reaction time to be 0.5-2 hours, carrying out washing and skimming after reaction is completed; adding a sodium carbonate solution to an organic phase to have hydrolysis, dispersing and concentrating the sodium carbonate solution after hydrolysis to obtain 4-cyclopentene-1,2,3-triketone. The preparation method is simple in process, easy to control, stable in reaction process and few in by-products and can be applied to high-voltage system employing a ternary material as a positive electrode.