161912-36-3Relevant articles and documents
Method for preparing pentafluorophenyl methanesulfonate at low cost
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Paragraph 0037-0040, (2019/02/13)
The invention discloses a method for preparing pentafluorophenyl methanesulfonate. The method comprises the following steps: dissolving pentafluorophenol in an organic solvent, and then adding an acidbinding agent to form a mixed solution; dropwise adding
Direct Synthesis of Sulfonamides and Activated Sulfonate Esters from Sulfonic Acids
Caddick, Stephen,Wilden, Jonathan D.,Judd, Duncan B.
, p. 1024 - 1025 (2007/10/03)
A general new method for the preparation of sulfonamides and activated sulfonate esters by the direct coupling of sulfonic acid salts with amines and alcohols using the reagent triphenylphosphine ditriflate is described. A new reusable polymer-supported reagent for these transformations under heterogeneous conditions is also described. These methods provide a fundamentally new approach to making small molecules containing the sulfonamide functional group. Copyright