166036-30-2Relevant academic research and scientific papers
Synthesis of 3,4-dihydro-3,3-dimethyl-1(2H)-acridinone
Martinez, Roberto,Espinosa-Perez, Georgina,Brito-Arias, Marco
, p. 201 - 204 (1995)
The acridinone derivative 3,4-dihydro-3,3-dimethyl-1(2H)-acridinone (4) has been prepared in a two step fashion and the molecular structure confirmed by X-ray diffraction.Compound 4 crystallizes in the space group P21/n with a = 6.022(2), b = 2
A three-component photoreversible tag for thiols
Clarke, Kristine M.,La Clair, James J.,Burkart, Michael D.
, p. 3709 - 3711 (2007/10/03)
(Chemical Equation Presented) A one-pot coupling of a 1,3-diketone, an aldehyde, and an alkanethiol has been developed to produce a protected sulfide. Through use of an o-nitrophenylbenzaldehyde, this method provides a one-step route to a photochemically reversible thiol-protecting group. The kinetics of photolysis were established using 1H NMR analysis, which allows for the rate to be based on the entire reaction scheme.
One pot facile synthesis of some new 9,10-dihydroacridine derivatives
Ahluwalia,Sahay, Ranjana,Das, Umashankar
, p. 1211 - 1213 (2007/10/03)
A convenient one pot synthesis of 9,10-dihydroacridine derivatives 3a-f and 4a-d has been described by the condensation of N-methylaniline or 5,5-dimethyl-3-benzylamino-2-cyclohexen-1-one with appropriate aromatic adehydes (1) and 5,5-dimethylcyclohexane-1, 3-dione (2) in methanol. These final products can alternatively be obtained from bis-dimedonyl derivatives (5) and 2-arylidene-5,5-dimethylcyclohexane-1,3-dione (6) on reaction with N-methylaniline or 5,5-dimethyl-3-benzylamino-2-cyclohexen-1-one and suggest the key steps to reaction mechanism.
