16794-67-5Relevant articles and documents
Synthesis, crystal structure, computational analysis and biological properties of 1-(4-chlorobenzoyl)-3-[2-(2-{2-[3-(4-chlorobenzoyl)-thioureido]-ethoxy}ethoxy)ethyl]-thiourea and its Ni(II) and Cu(II) complexes
Oyeka, Ebube Evaristus,Asegbeloyin, Jonnie Niyi,Babahan, Ilknur,Eboma, Bernard,Okpareke, Obinna,Lane, Joseph,Ibezim, Akachukwu,B?y?k, H. Halil,T?rün, Bahad?r,Izuogu, David Chukwuma
, p. 153 - 164 (2018)
A new dianionic ligand, 1-(4-chlorobenzoyl)-3-[2-(2-{2-[3-(4-chlorobenzoyl)-thioureido]-ethoxy}ethoxy)ethyl]-thiourea(CBEDEA), and its Ni(II) and Cu(II) complexes have been synthesized. X-ray single crystal analysis of CBEDEA shows that the molecule cryst
Synthesis and Investigation of the Antibacterial Activity of New Tris-Thiourea Derivatives
Ghorbani, Saghi Shiroud,Montazeri, Naser,Zeydi, Masoud Mohammadi,Ghane, Masood
, p. 60 - 64 (2021)
An efficient procedure for the preparation of symmetrical tris-thiourea derivatives (5a – 5h) by means of one-pot condensation reaction between available benzoyl chlorides (1a –1h) with potassium thiocyanate (2) and melamine (4) under reflux conditions is
Caffeine catalyzed green synthesis of novel benzo[a][1,3]oxazino[6,5-c]phenazines via a one-pot multi-component sequential protocol in a basic ionic liquid
Mohebat, Razieh,Yazdani-Elah-Abadi, Afshin
, p. 1340 - 1344 (2017)
Caffeine was applied as a green and natural catalyst for the one-pot, four-component sequential condensation between 2-hydroxy-1,4-naphthoquinone, aromatic 1,2-diamines, ammonium thiocyanate and acid chlorides in the presence of a basic ionic liquid (1-butyl-3-methylimidazolium hydroxide) to afford the corresponding benzo[a][1,3]oxazino[6,5-c]phenazine derivatives. In this one-pot transformation, five bonds and two new rings are efficiently formed. This protocol has the advantages of operational simplicity, high yields, easy workup, avoidance of hazardous or toxic catalysts and organic solvents and high chemo- and regioselectivities.
One-pot solvent-free synthesis of novel functionalized ethyl 2-(alkylimino)-4-methyl-3-(alkanoyl)-2,3-dihydrothiazole-5-carboxylates
Iravani, Nasir,Keshavarz, Mosadegh,Hosseini, Fatemeh
, p. 1098 - 1103 (2018)
A green and efficient one-pot two-step synthesis of ethyl 2-(alkylimino)-4-methyl-3-(alkanoyl)-2,3-dihydrothiazole-5-carboxylates from the reaction between acyl chlorides, ammonium thiocyanate, primary alkylamines, and ethyl 2-chloroacetoacetae under mild
Synthesis, Characterization, and Structural Investigations of 1-(3-morpholinopropyl)-3-(4-chlorobenzoyl)thiourea monohydrate and 1-(3-morpholinopropyl)-3-(4-methylbenzoyl)thiourea monohydrate
Razak, Ibrahim Abdul,Arshad, Suhana,Thanigaimani, Kaliyaperumal,Yusof, Mohd Sukeri Mohd,Abdullah, Sharifah Sakinah,Rahman, Azhar Abdul
, p. 151 - 175 (2015)
Two new compounds, 1-(3-morpholinopropyl)-3-(4-chlorobenzoyl)thiourea monohydrate (I) and 1-(3-morpholinopropyl)-3-(4-methylbenzoyl)thiourea monohydrate (II) have been synthesized and characterized by FT-IR, 1H NMR, 13C NMR, and Sing
A PROCESS FOR PREPARING 2-CHLORO-N-{[4-(PYRIMIDIN-2-YLSULFAMOYL)PHENYL] CARBAMOTHIOYL} BENZAMIDE AND THE PHARMACEUTICAL UTILITY THEREOF
-
Page/Page column 8; 9, (2021/07/10)
Disclosed is a process for preparing 2-chloro-N-{[4-(pyrimidin-2-ylsulfamoyl)phenyl] carbamothioyl} benzamide (compound 2c).
Synthesis of Novel Tris-1,2,4-triazole Derivatives and Their Antibacterial Activity
Ghane, M.,Ghorbani, S. Shiroud,Montazeri, N.,Zeydi, M. M.
, p. 605 - 610 (2021/06/02)
Abstract: A series of novel 3,3′,3″-[1,3,5-triazine-2,4,6-triyltris(azanediyl)]tris(5-aryl-1H-1,2,4-triazole-1-carbothioamide) derivatives were designed and synthesized through reaction of new tris-thiourea derivatives with thiosemicarbazide and sodium hy