17588-45-3

Basic information

• Product Name: 4-[(2,6-dimethylphenyl)diazenyl]-3,5-dimethylphenol
• Synonyms: 4-[(2,6-dimethylphenyl)diazenyl]-3,5-dimethylphenol
• CAS NO: 17588-45-3
• Molecular Formula: C16H18N2O
• Molecular Weight: 254.32692
• Mol File: 17588-45-3.mol
• Article Data: 1

Chemical Properties

• Appearance: /
• CAS DataBase Reference: 4-[(2,6-dimethylphenyl)diazenyl]-3,5-dimethylphenol(CAS DataBase Reference)
• NIST Chemistry Reference: 4-[(2,6-dimethylphenyl)diazenyl]-3,5-dimethylphenol(17588-45-3)
• EPA Substance Registry System: 4-[(2,6-dimethylphenyl)diazenyl]-3,5-dimethylphenol(17588-45-3)

Safety Data

• Hazardous Substances Data: 17588-45-3(Hazardous Substances Data)

Relevant articles and documents

Synthesis method and application of novel p-aryl azophenol derivative

The invention provides a synthesis method of a p-aryl azophenol derivative. The synthesis method comprises the following step of: subjecting two aryl diazonium salts serving as raw materials to reacting in a mixed solvent of water under the action of an additive to generate the p-aryl azophenol derivative with a structure as shown in a formula (I) that is described in the specification. The chemical structure of the diazonium salt is as described in the specification, and in the chemical structure, R and R1 groups are selected from straight-chain or branched-chain alkyl groups, straight-chain alkoxy groups, halogen, nitryl groups, ester groups, trifluoromethyl groups and cyano groups. The additive is one or more selected from a group consisting of lithium acetate, sodium acetate, potassium acetate, cesium acetate, sodium carbonate, triethylamine, N,N-diisopropylethylamine, diazabicyclo and potassium tert-butoxide. The solvent is one or more selected from the group consisting of benzyl alcohol, acetonitrile, methanol, ethanol, acetone and water. According to the invention, a one-pot cascade reaction of aryl diazonium salt and water is realized under mild and transition metal-free conditions, and the multifunctional p-substituted azophenol derivative is conveniently and efficiently synthesized.