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185147-06-2

185147-06-2

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185147-06-2 Usage

Chemical Properties

Off-white crystalline

Check Digit Verification of cas no

The CAS Registry Mumber 185147-06-2 includes 9 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 6 digits, 1,8,5,1,4 and 7 respectively; the second part has 2 digits, 0 and 6 respectively.
Calculate Digit Verification of CAS Registry Number 185147-06:
(8*1)+(7*8)+(6*5)+(5*1)+(4*4)+(3*7)+(2*0)+(1*6)=142
142 % 10 = 2
So 185147-06-2 is a valid CAS Registry Number.
InChI:InChI=1/C8H6FN/c1-6-7(5-10)3-2-4-8(6)9/h2-4H,1H3

185147-06-2 Well-known Company Product Price

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  • Alfa Aesar

  • (H26413)  3-Fluoro-2-methylbenzonitrile, 97%   

  • 185147-06-2

  • 1g

  • 1159.0CNY

  • Detail

  • Alfa Aesar

  • (H26413)  3-Fluoro-2-methylbenzonitrile, 97%   

  • 185147-06-2

  • 5g

  • 3566.0CNY

  • Detail

185147-06-2SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 16, 2017

Revision Date: Aug 16, 2017

1.Identification

1.1 GHS Product identifier

Product name 3-Fluoro-2-methylbenzonitrile

1.2 Other means of identification

Product number -
Other names 3-fluoro-2-methylbenzenecarbonitrile

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:185147-06-2 SDS

185147-06-2Relevant articles and documents

Transnitrilation from Dimethylmalononitrile to Aryl Grignard and Lithium Reagents: A Practical Method for Aryl Nitrile Synthesis

Reeves, Jonathan T.,Malapit, Christian A.,Buono, Frederic G.,Sidhu, Kanwar P.,Marsini, Maurice A.,Sader, C. Avery,Fandrick, Keith R.,Busacca, Carl A.,Senanayake, Chris H.

supporting information, p. 9481 - 9488 (2015/08/11)

An electrophilic cyanation of aryl Grignard or lithium reagents, generated in situ from the corresponding aryl bromides or iodides, by a transnitrilation with dimethylmalononitrile (DMMN) was developed. DMMN is a commercially available, bench-stable solid. The transnitrilation with DMMN avoids the use of toxic reagents and transition metals and occurs under mild reaction conditions, even for extremely sterically hindered substrates. The transnitrilation of aryllithium species generated by directed ortho-lithiation enabled a net C-H cyanation. The intermediacy of a Thorpe-type imine adduct in the reaction was supported by isolation of the corresponding ketone from the quenched reaction. Computational studies supported the energetic favorability of retro-Thorpe fragmentation of the imine adduct. (Chemical Equation Presented).

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