18557-58-9Relevant academic research and scientific papers
Triphenylsilyl Perchlorate Revisited: 29Si and 35Cl NMR Spectroscopy and X-ray Crystallography Showing Covalent Nature in Both Solution and the Solid State. Difficulties in Observing Long-Lived Silyl Cations in the Condensed State
Prakash, G. K. Surya,Keyaniyan, Schahab,Aniszfeld, Robert,Heiliger, Ludger,Olah, George A.,et al.
, p. 5123 - 5126 (1987)
29Si and 35Cl NMR spectroscopic and X-ray crystallographic study of triphenylsilyl perchlorate shows it to be a covalent perchloryl ester in both solution and the solid state.The results are in accord with earlier studies notably those of Wannagat but con
Continued search for elusive persistent trivalent organosilyl cations: The claimed trimethylsilyl cation revisited. Attempted preparation of cyclic and halogen-bridged organosilicenium ions
Olah, George A.,Rasul, Golam,Heiliger, Ludger,Bausch, Joseph,Surya Prakash
, p. 7737 - 7742 (2007/10/02)
Comparison of ab initio/IGLO calculated 1H, 13C, and 29Si NMR chemical shifts with the experimental data on trimethylsilyl perchlorete and related derivatives supports the conclusion that no long-lived persistent trimethyl
