187845-78-9Relevant articles and documents
Microwave-assisted cross-coupling for the construction of diaryl sulfides
Tan, Chen-Ming,Chen, Grace Shiahuy,Chena, Chien-Shu,Chern, Ji-Wang
, p. 94 - 100 (2011)
The construction of diaryl sulfides through the cross-coupling of aryl iodides and thiols in microwave heating is described. By using this method, a variety of diaryl sulfides can be prepared in a mild condition and in high yields. Deactivated 4-nitrothiophenol was effective to afford the product in 94% yield. Sterically hindered ortho-substituted aryl iodides or thiophenols provided diaryl sulfides effectively by this microwave-assisted coupling reaction.