18959-30-3Relevant articles and documents
High-efficiency synthesis method of halogenated 1, 3-indanedione compound
-
Paragraph 0028-0030, (2020/08/09)
The invention relates to the technical field of new material synthesis, in particular to a novel efficient synthesis method of an organic photoelectric intermediate material. The method is characterized in that the synthesis technology is simple, efficient, easy to operate and good in repeatability. The specific synthesis details are as follows: halogenated phthalic acid which is very easy to obtain in industry is used as a raw material, and a corresponding anhydride is obtained after dehydration treatment; different acid anhydrides are reacted with ethyl acetoacetate or tert-butyl acetoacetate at room temperature, and then carboxyl is mildly removed in a hydrochloric acid aqueous solution to obtain the halogenated 1, 3-indanedione compound. Simple and efficient synthesis of the organic intermediates is achieved through the method, synthesis raw materials are easy to obtain, the synthesis process is simple, the path is short, and the synthesis cost is greatly reduced.
Intermediates in the preparation of 4,5-difluoroanthranillic acid
-
, (2008/06/13)
Compounds of the formula STR1 which are intermediates in the preparation of 4,5-difluoroanthranilic acid, an intermediate itself in the synthesis of quinolone antibacterials, and methods of preparing these intermediates.