200407-55-2Relevant academic research and scientific papers
Continuous flow iodination using an automated computer-vision controlled liquid-liquid extraction system
O'Brien, Matthew,Cooper, Dennis A.,Dolan, Jonathan
supporting information, p. 829 - 834 (2017/02/10)
A dynamic computer-vision control system incorporating open-source software technologies (Python, OpenCV) was used to automate a gravity based in-line liquid-liquid extraction during the iodination of enaminones in continuous flow. The system was able to cope with significant colouration of the organic reaction stream and with significant volume/flow changes in the aqueous and organic phase streams due to extraction of the water soluble acetonitrile co-solvent.
α-Iodination of enaminones using the modified Johnson's procedure: The use of I2 and Et3N
Kim, Jeong Mi,Na, Jeong Eun,Kim, Jae Nyoung
, p. 6317 - 6318 (2007/10/03)
Facile synthesis of α-iodo enaminones 2 was carried out by the use of iodine and triethylamine in methylene chloride in short time in excellent yields.
α-Iodination of enaminones with bis(pyridine)iodonium(I) tetrafluoroborate
Campos, Pedro J.,Arranz, Joaquin,Rodriguez, Miguel A.
, p. 8397 - 8400 (2007/10/03)
Primary, secondary and tertiary enaminones react with bis(pyridine)iodonium(I) tetrafluoroborate in methylene chloride at room temperature to give α-iodo enaminones in almost quantitative yields. The reported reaction is the fast known example of direct iodination of tertiary enaminones.
