20850-80-0Relevant academic research and scientific papers
3,5-Diphenyl-1,2-dithiolium Hydrogensulphate - Synthesis and Structure
Uhlemann, Erhard,Weller, Frank
, p. 1501 - 1504 (2007/10/02)
3,5-Diphenyl-1,2-dithiolium hydrogensulphate was prepared by the reaction of bis(thiodibenzoylmethanato)-nickel (II) with thionyl chloride in acetonitrile solution.The compound was characterized by X-ray structure determination (1261 observed, independent reflexions, R = 0.056).Crystal data: a = 543.1(1), b = 1605.7(1), c = 1678.9(2) pm; space group P212121, Z = 4.By hydrogen bonding the hydrogensulphate ions form chains of weakly helical structure.Key words: 3,5-Diphenyl-1,2-dithiolium Hydrogensulphate, Synthesis, Crystal Structure, Bis(thiodibenzoylmethanato)-nickel(II), Thionyl Chloride
