22047-49-0Relevant articles and documents
Preparation method of low-polarity grease
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Paragraph 0067; 0068; 0069, (2018/06/16)
The invention relates to the fields of fine chemical products, and particularly provides a preparation method of low-polarity grease. The method comprises the following steps: performing contact reaction between acyl chloride and fatty alcohol in the presence of a solvent and an acid binding agent, and performing separation to obtain a grease product. The synthetic method provided by the inventionenables the fatty alcohol and the acyl chloride to be subjected to nucleophilic substitution reaction which does not have reverse reaction (a by-product is hydrochloric acid), the reaction yield of the nucleophilic substitution reaction is generally higher than that of general esterification reaction, the process is simple, reaction conditions are mild, and the final yield is as high as 80%. Themethod provided by the invention can be used for preparing colorless and tasteless products which are easy to store and good in stability.