2227-40-9Relevant academic research and scientific papers
Novel method for preparing phosphoryl azo compound (by machine translation)
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Paragraph 0007; 0013, (2020/12/15)
The method adopts pyridine as a base, takes an aryl diazonium tetrafluoroborate compound and P (O)- H as a reaction substrate, and an organic solvent is added to the reaction system. The method has the advantages that the catalyst is cheap and easy to obtain. The substrate applicability is high. The reaction condition is mild, safe and reliable. The selectivity of the obtained target product is close 100%, and the yield is high. The method solves the harsh reaction conditions of the traditional synthetic phosphoryl azo compound. The reaction selectivity is poor, the experiment steps are tedious, the yield is low and the harmful reagents and the like on the environment are required to be used, and the industrial application prospect is good. The invention also provides a corresponding phosphoryl azo compound containing different substituted functional groups. (by machine translation)
