22364-91-6Relevant articles and documents
Contributions to the Chemistry of Boron. Part 160. A Convenient Synthesis of Catecholatoborane and Diborane
Maennig, Detlef,Noeth, Heinrich
, p. 1689 - 1692 (1985)
Catecholatoborane is formed in high yield (> 75percent) by ball milling NaBH4 and 2,2'-o-phenylenedioxybis(1,3,2-benzodioxaborole) in diethyl ether in the presence of small amounts of LiCl.It also results quantitatively from the first two components in di