2253-54-5Relevant articles and documents
Microwave irradiation technique for synthesis of dialkyl dithiophosphoric acids
Guemguem, Bahattin,Biricik, Nermin,Baysal, Akin
, p. 2507 - 2512 (2007/10/03)
Microwave heating technique was applied to the preparation of dialkyl dithiophosphoric acids from the reaction of alcohol with phosphorus pentasulphide. A microwave oven (CEM-MDS 2000) was utilized to determine the preparation conditions for the best yield of dialkyl dithiophosphoric acids under atmospheric pressure at various times and power. Six different (C4-C9) chain-length of dialkyl dithiophosphoric acids were studied. All experiments were performed in an open Teflon (poly-tetrafluoroethylene) vessel. The results obtained showed that the reaction of dialkyl dithiophosphoric acids can be achieved more rapidly using microwave heating than using conventional procedures.
REACTION OF THE SODIUM DERIVATIVE OF MALONONITRILE WITH BIS(DIPHENYLOXYPHOSPHINOTHIOYL) DISULFIDE
Khaskin, B. A.,Rymareva, T. G.,Sandakov, V. B.
, p. 2358 - 2359 (2007/10/02)
-
REACTIONS OF ALIPHATIC ALCOHOLS WITH SULFUR AND RED PHOSPHORUS
Mazitova, F. N.,Khairullin, V. K.
, p. 1393 - 1396 (2007/10/02)
-