23843-64-3Relevant academic research and scientific papers
METHOD FOR PRODUCING UREIDO GROUP-CONTAINING ORGANOSILICON COMPOUND
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Paragraph 0066-0084, (2020/03/28)
A method for producing an ureido group-containing organosilicon compound includes the following steps (I) and (II): (I): a step of obtaining a compound represented by formula (1) by reacting urea and an amino group-containing organosilicon compound represented by formula (3): wherein R1 represents an alkyl group having 1 to 10 carbon atoms or the like, R3 represents a hydrogen atom or the like, Me represents a methyl group, m represents an integer of 1 to 3, and n represents an integer of 1 to 12, wherein R2 represents a hydrogen atom or the like, and R1, Me, m, and n represent the same meaning as described above; and (II): a step of further reacting by supplying the amino group-containing organosilicon compound represented by formula (3) to a mixture containing a compound represented by formula (1) and urea.
Process for manufacturing polysiloxane microcapsules that are functionalized and are not very porous
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Page/Page column 3, (2016/09/26)
A method is provided for encapsulating products that can have lipophilic or hydrophilic, including volatile, properties in a polysiloxane membrane that is particularly impervious. A method is also provided for evaluating the imperviousness of capsules. The present method includes the following steps: a) formation of droplets by an emulsion between an oily phase containing the product to be encapsulated and an acidic aqueous phase heated to around 50° C. and in the presence of surfactants; b) addition and hydrolysis of at least one silane in order to obtain a silanol; c) increasing the pH in order to start condensation of the silanol to form a first membrane around the droplets of the product to be encapsulated; d) lowering the pH; e) increasing the pH, optionally preceded by adding a silane, in order to obtain a new condensation of silanol around the droplets of the product to be encapsulated.
