2418-14-6Relevant articles and documents
Dimercaptosuccinic acid and salt thereof and preparation method
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Paragraph 0171; 0172; 0173; 0174, (2018/03/28)
The invention relates to the technical field of organic synthesis, in particular to dimercaptosuccinic acid and salt thereof and a preparation method. The preparation method comprises the following steps: carrying out reaction on ethyl xanthate and 2,3-dibromosuccinic acid, so that 2,3-diethyl xanthate-1,4 succinic acid is obtained; hydrolyzing the 2,3-diethyl xanthate-1,4 succinic acid, so that 2,3-dimercaptosuccinate solution is obtained; and acidifying the obtained 2,3-dimercaptosuccinate solution, so that 2,3-dimercaptosuccinic acid is obtained. The preparation method provided by the invention has the advantages that technology is simple, liquid-state thioacetic acid with strong odor and unstable quality does not need to be used, unsafe addition reaction does not need to be carried out, preparation period is short, yield is high, cost is low, and the dimercaptosuccinic acid can be applicable to industrial production and popularization and can be further prepared into a dimercaptosuccinate product. The dimercaptosuccinic acid product and the dimercaptosuccinate product are high in purity and low in cost.