244067-02-5Relevant articles and documents
Synthesis, high-field NMR, X-ray structure, and conformational analysis of a 10-membered diamide disulfide ring
Maharajh, Rabindranath B.,Snyder, James P.,Britten, James F.,Bell, Russell A.
, p. 140 - 161 (1997)
N,N′-[Dimethyl-(2,2′-dithiobisacetyl)]ethylenediamine (1) has been synthesized in 30% overall yield from N,N′-dimethylethylenediamine and thioacetic acid by an improved procedure involving simultaneous deprotection and oxidative cyclization with iodine. T
NMR studies of chemical exchange amongst five conformers of a ten-membered ring compound containing two amide bonds and a disulfide
Bain, Alex D.,Bell, Russell A.,Fletcher, Daniel A.,Hazendonk, Paul,Maharajh, Rob A.,Rigby, Suzie,Valliant, John F.
, p. 1447 - 1453 (2007/10/03)
This paper presents experimental measurements which provide a very detailed picture of the free energy surface of a molecule. The compound, N,N′-dimethyl-N′,N′-(2,2′-dithiobisacetyl) ethylenediamine (a diamino-disulfide, DADS, chelate), is a symmetrical t