252921-82-7

Basic information

• Product Name: 3-Cyclohexene-1-methanamine, 1,5,5-trimethyl-
• Synonyms: 3-Cyclohexene-1-methanamine, 1,5,5-trimethyl-
• CAS NO: 252921-82-7
• Molecular Formula: C10H19N
• Molecular Weight: 153.26
• Mol File: 252921-82-7.mol
• Article Data: 1

Chemical Properties

• Appearance: /
• CAS DataBase Reference: 3-Cyclohexene-1-methanamine, 1,5,5-trimethyl-(CAS DataBase Reference)
• NIST Chemistry Reference: 3-Cyclohexene-1-methanamine, 1,5,5-trimethyl-(252921-82-7)
• EPA Substance Registry System: 3-Cyclohexene-1-methanamine, 1,5,5-trimethyl-(252921-82-7)

Safety Data

• Hazardous Substances Data: 252921-82-7(Hazardous Substances Data)

Upstream product

• 72641-10-2 3-cyano-3,5,5-trimethylcyclohexanol O-methanesulfonate 
• 7027-11-4 isophoronenitrile 
• 72641-05-5 5-hydroxy-1,3,3-trimethylcyclohexanecarbonitrile 
• 78-59-1 3,5,5-Trimethylcyclohex-2-en-1-one 

Relevant articles and documents

Synthesis of 3H-labeled 2-hydroxy-N-[(1,3,3-trimethyl-[4,5,6-3H]cyclohexyl)methyl]-5-azidobenzamide, a photoaffinity analog of an influenza fusion inhibitor

Synthesis of 3H-labeled 2-hydroxy-N-[(1,3,3-trimethyl-[4,5,6-3H]cyclohexyl)methyli]-5-azidobenzamide, a photoaffinity analog of an influenza fusion inhibitor, is reported. Tritiation of a mixture of N-(t-butoxycarbonyl)-1,3,3-trimethylcyclohex-4 (or 5)-enylmethylamine via T2 and Pd/C, followed by coupling of the deprotected tritiated amine with acetyl 5-azidosalicylic acid chloride yielded the penultimate product. Subsequent deprotection and normal phase HPLC purification yielded the target compound with a radiochemical purity > 99% and a specific activity of 63 Ci/mmol.