259881-39-5Relevant articles and documents
Preparation method for 9,9-bis[4-(2,3 epoxy propoxy ethyoxyl)phenyl]fluorene
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Paragraph 0008; 0022-0029, (2017/04/11)
The invention relates to a preparation method of 9,9-bis[4-(2,3 epoxy propoxy ethyoxyl)phenyl] fluorene. The preparation method specifically comprises the step of enabling raw materials 9,9-bis[4-(2-hydroxyethoxy)phenyl]fluorene and epichlorohydrin to react in the presence of sodium hydroxide and anhydrous calcium chloride. The preparation method of 9,9-bis[4-(2,3 epoxy propoxy ethyoxyl)phenyl] fluorene, provided by the invention, has the advantages of not using organic solvents, having fewer side reactions during the reaction, being high in yield, simple in operation, environmentally friendly and the like, thereby being suitable for industrial production.
EPISULFIDE COMPOUND HAVING A FLUORENE SKELETON AND CURED PRODUCT THEREOF
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Paragraph 0115, (2017/05/10)
PROBLEM TO BE SOLVED: To provide a compound which can provide a cured product having excellent properties such as high heat resistance and high refractive index. SOLUTION: The present invention provides an episulfide compound represented by formula (1) (where, ring Z is a condensed polycyclic aromatic hydrocarbon ring such as a naphthalene ring; R1 is H or a substituent; R2 is an alkylene group; R3 is a substituent; k is an integer of 0-4, m is 1, n is an integer of 0 or more). Preferably Z is a naphthalene ring in the episulfide compound. SELECTED DRAWING: None COPYRIGHT: (C)2017,JPOandINPIT