2620-27-1Relevant articles and documents
Method for separating N,N,N'-trimethylbisaminoethylether and/or N,N-dimethylbisaminoethylether from a mixture
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Paragraph 0159; 0160; 0161; 0162, (2015/05/05)
The present invention relates to a method for separating N,N,N'-trimethylbisaminoethylether and/or N,N-dimethylbisaminoethylether, from a mixture A comprising N,N,N'-trimethylbisaminoethylether, and N,N-dimethylbisaminoethylether, wherein said method comprises the steps of: (a) contacting said mixture A with an acylating agent, to form a mixture B comprising the amides of N,N,N'-trimethylbisaminoethylether and of N,N-dimethylbisaminoethylether, respectively; and (b1) separating the amide of N,N,N'-trimethylbisaminoethylether from mixture B; and (c1) recovering N,N,N'-trimethylbisaminoethylether from its amide by means of a transamidation reaction; and/or (b2) separating the amide of N,N-dimethylbisaminoethylether from mixture B; and (c2) recovering N,N-dimethylbisaminoethylether from its amide by means of a transamidation reaction.
MACROHETEROCYCLES. XVI. SYNTHESIS OF MACROCYCLIC LACTONOLACTAMS AND THEIR ION-SELECTIVE CHARACTERISTICS
Bogat-skii, A.V.,Luk'yanenko, N.G.,Shapkin, V.A.,Popkov, Yu.A.,Nazarova, N.Yu.,Chernotkach, Z.A.
, p. 798 - 804 (2007/10/02)
Sewenteen new macrocyclic lactonolactams were obtained by the acylation of N,N'-dimethylpolyoxyalkanediamines with acid dichlorides in benzene under conditions of high dilution.The coefficients of cationic selectivity in the series of alkali and alkaline-earth metals were determined for them, and compounds which exhibit high calcium selectivity were found.