28251-63-0Relevant articles and documents
A suitable for industrial production process for the separation of chemical synthesis salidroside
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Paragraph 0024-0026; 0030-0032; 0035-0037; 0040-0042, (2019/02/04)
The invention discloses a separation method suitable for chemical synthesis of salidroside for industrial production. The method comprises the following steps: carrying out a reaction on Beta-D-pent-acetyl glucose and hydroxyphenethyl alcohol under the catalytic action of a lewis acid; and carrying out deacetylation on a generated tetraacetyl salidroside product so as to prepare the salidroside. Thus, the salidroside product is synthesized in a separating manner via an extraction and recrystallization method while a simple and convenient synthesis method is adopted at the same time. Compared with the traditional chemical synthesis process, the method disclosed by the invention is low in cost, high in yield, short in reaction time, simple and simple, convenient and environmentally friendly in synthesis process, thereby being suitable for industrial production, and the raw materials are easily available.
Synthesis of 13C-labeled possible intermediates in the biosynthesis of phenylethanoid derivatives, cornoside and rengyosides
Kuwajima, Hiroshi,Takai, Yoshitaka,Takaishi, Kiyokazu,Inoue, Kenichiro
, p. 581 - 586 (2007/10/03)
In order to clarify the biosynthetic pathway of C6-C2 unit compounds containing salidroside, cornoside, and rengyosides A and B in oleaceous plants, 13C-labeled putative precursors, 4-hydroxyphenylethanol, salidroside and cornoside, were prepared.
Aryl β-d-glucosides from Carica papaya fruit
Schwab, Wilfried,Schreier, Peter
, p. 1813 - 1816 (2007/10/02)
Benzyl β-d-glucoside, 2-phenylethyl β-d-glucoside, 4-hydroxyphenyl-2-ethyl β-d-glucoside and four isomeric malonated benzyl β-d.