291782-01-9Relevant academic research and scientific papers
6,6'-Dibromo-3,3'-dimethoxy-2,2'-dihydroxy-1,1'-biphenyl: Preparation and resolution
Delogu, Giovanna,Fabbri, Davide,Dettori, Maria Antonietta,Casalone, Gianluigi,Forni, Alessandra
, p. 1827 - 1833 (2007/10/03)
A pratical route to prepare the title biphenyl 1 starting from 3,3',2,2'-tetramethoxy-1,1'-biphenyl 2 is described. Resolution of 1 was achieved by its conversion into the corresponding diastereomeric menthyldicarbonate. The absolute configuration of (P)-(+)-1 was confirmed by X-ray analysis of the related diastereomer. (C) 2000 Elsevier Science Ltd.
