30221-55-7Relevant articles and documents
Expeditious microwave-assisted thionation with the system PSCl 3/H2O/Et3N under solvent-free condition
Pathak, Uma,Pandey, Lokesh Kumar,Tank, Rekha
, p. 2890 - 2893 (2008/09/19)
(Chemical Equation Presented) A novel thionation protocol for carbonyl compounds, with the system PSCl3/H2O/Et3N has been discovered. Clean, rapid, and efficient synthesis of a variety of thiocarbonyl compounds such as thioamides, thiolactams, thioketones, thioxanthones, and thioacridone can be achieved through this simple and convenient method under solventless condition with microwave irradiation.
Bis(trimethylsilyl)sulfide based thionation of carbonyl compounds: Synthesis of thioketones
Degl'Innocenti,Capperucci,Mordini,Reginato,Ricci,Cerreta
, p. 873 - 876 (2007/10/02)
A wide range of thioketones may be conveniently obtained by silyl triflate promoted bis(trimethylsilyl)sulfide thionation of ketones.