3046-50-2Relevant articles and documents
Synthesis of N-(2,3-dihydro-1-[14C]methyl-2-oxo-5-phenyl-1H-1, 4-benzodiazepin-3-yl)-benzamide and N-(2,3-dihydro-1-[14C]methyl-2-oxo-5-phenyl-1H-1, 4-benzodiazepin-3-yl)-N-[14C]methyl-benzamide as novelcarbon-14 labelled CCK antagonists
Matloubi, Hojatollah,Khalaj, Ali,Dowlatabadi, Reza,Shirvani, Gholamhossein
, p. 347 - 350 (2007/10/03)
Two benzodiazepine CCK antagonists N-(2,3-dihydro-1-[14C]methyl-2-oxo-5-phenyl-1H 1,4-benzodiazepin-3-yl)-benzamide 2 and N-(2,3-dihydro-1-[14C]methyl-2-oxo-5-phenyl-1H-1, 4-benzodiazepin-3-yl)-[14C]methyl-benzamide 3 were synthesized in high yields through the reaction of N-(2,3-dihydro-2-oxo-5-phenyl-1H-1,4-benzodiazepin-3-yl)-benzamide 1 with [14C] methyl iodide in different situations. Copyright
Determination of Heavy-Atom Kinetic Isotope Effects by Liquid Scintillation Spectrometry with Internal Standardisation. Kinetic Isotope Effects in the Reaction of Pyridine with Methyl Iodide and in the Reaction of N,N-Dimethylaniline Methiodide with Hydroxide Ion.
Husain, Syed M.,McKenna, James,McKenna, Jean M.
, p. 3612 - 3623 (2007/10/02)
The use of a liquid scintillation spectrometer as the basis of a convenient method for determining heavy-atom kinetic isotope effects is described in detail.The method is illustrated by measurement of isotope effects for the reaction of pyridine with methyl iodide in benzene, and for the decomposition of N,N-dimethylaniline methiodide with aqueous potassium hydroxide.