35583-12-1Relevant academic research and scientific papers
Synthesis of diacetals of 2,2-bis(hydroxymethyl)1,3-propanediol under microwave irradiation
Wang, Cun-De,Shi, Xin-Zhong,Xie, Ren-Jian
, p. 2517 - 2520 (1997)
Nine diacetals (3a-i) of 2,2-bis(hydroxymethyl)-1,3-propanediol (2) were prepared by condensation of aldehydes with 2 under microwave irradiation in the presence of TsOH without solvent.
Acetalization of carbonyl compounds as pentaerythritol diacetals and diketals in the presence of cellulose sulfuric acid as an efficient, biodegradable and reusable catalyst
Shaterian, Hamid Reza,Rigi, Fatemeh
experimental part, p. 695 - 698 (2012/05/05)
This paper reports a practical and green method for the acetalization of carbonyl compounds as pentaerythritol diacetals and diketals derivatives using cellulose sulfuric acid as a biodegradable and reusable solid acid catalyst under thermal solvent-free conditions.
Synthesis of diacetals from aldehydes and ketones with pentaerythritol catalysed by the ZrO2/S2O82- solid superacid
Jin, Tongshou,Yang, Mina,Wang, Xin,Feng, Guoliang,Li, Tongshuang
, p. 203 - 205 (2007/10/03)
A manipulatively simple and rapid procedure for the synthesis of diacetals from 2,2-bis(hydroxymethyl)-1, 3-propanediol with aldehydes and ketones in refluxing benzene or toluene using the ZRO2/S2O 82- solid superacid as catalyst in 80-98% yields has been described.
An efficient procedure for the synthesis of diacetals from the InCl3·4H2O catalysed reaction of 2,2-bis (hydroxymethyl)-1,3-propanediol with aldehydes or ketones
Deng, Guisheng,Ren, Tiegan
, p. 24 - 25 (2007/10/03)
Diacetals of carbonyl compounds are synthesised in good yields by the InCl3·4H2O catalysed condensation reactions.
Microwave-assisted acetalization of pentaerythritol catalyzed by 12-tungstophosphoric acid
Peng,Song,Qian
, p. 3735 - 3738 (2007/10/03)
Efficient conversion of carbonyl compounds and pentaerythritol to corresponding diacetals in the presence of 12-tungstophosphoric acid under microwave irradiation is described.
