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A new synthetic approach to N,N′-disubstituted 1,n-alkanediamines
Orelli,Blanco,Garcia,Hedrera,Perillo
, p. 685 - 695 (2007/10/03)
A general procedure is described for the synthesis of unsymmetrically substituted N-aryl-N′-alkyl (or aryl) 1,n-alkanediamines 1 (n = 2-5) by reduction of ω-alkyl (or aryl) aminoalkanamides 2 with borane. Compounds 2 are easily obtained by aminolysis of the corresponding ω-haloalkanamides 3.
