3693-94-5Relevant academic research and scientific papers
A novel method for the synthesis of thioacetates using benzyltriethyl- ammonium tetrathiomolybdate and acetic anhydride
Nasir, Baig R. B.,Sai, Sudhir V.,Srinivasan, Chandrasekaran
scheme or table, p. 2684 - 2688 (2009/04/16)
Herein we report a simple and efficient methodology for the synthesis of thioacetates using benzyltriethylammonium tetrathiomolybdate and acetic anhydride as the key reagents, starting from alkyl halides in a multistep, tandem reaction process. Its application in the synthesis of orthogonally protected cysteine and anomeric β-thioglycosides has also been demonstrated.
