39562-20-4Relevant articles and documents
Synthesis of [allyl-2,3-3H]-MN-9201
Wu, Dezhu,Huang, Wenlin,Wang, Wen,Mei, Qibing
, p. 785 - 789 (2007/10/03)
Key step of the synthesis of calcium antagonist MN-9201 was the cyclizing addition of the ally-13-amino-crotonate onto methyl 2-[(3- nitrophenyl) methylene ]-3-oxobutanoate. It was then used to synthesize [Allyl-2,3-3H]-MN-9201 by the catalytic addition of tritium gas. Its radiochemical purity and specific activity were 98% and 2.1TBq/mmol, respectively.