401649-83-0Relevant academic research and scientific papers
Synthesis and transformations of 3-acetylpyridine-2(1H)-thiones
Zav'Yalova,Zubarev,Litvinov
experimental part, p. 1534 - 1538 (2009/10/01)
Reactions of substituted 3-cyanopyridine-2(1H)-thiones with methyllithium gave 3-acetylpyridine-2(1H)-thiones. The best results were achieved by adding a solid-state thione to a solution of methyllithium in ether (thione: MeLi = 1: 3). The compounds obtained and their 3-pentanoyl analogs were used to synthesize a number of fused heterocyclic systems.
