40599-01-7Relevant academic research and scientific papers
DCDMH-promoted synthesis of thiophosphates by coupling of H-phosphonates with thiols
Bi, Xiaojing,Li, Junchen,Meng, Fanhua,Wang, Hongmei,Xiao, Junhua
, p. 706 - 711 (2016)
DCDMH-mediated phosphorylation of versatile thiols with H-phosphonates for the preparation of synthetically and biologically important thiophosphates was demonstrated. Without metal catalysts and other additives, phosphorylation occurred to give the desired products with good to excellent yields within 10 min at ambient temperature in the air.
A thiophosphate synthetic method of compound
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Paragraph 0033; 0034; 0035; 0036; 0037; 0038-0042; 0118-0122, (2017/09/01)
The present invention relates to a synthetic method of phosphorothioate compound. The preparation method adopts phosphite and thiophenol or mercaptan to synthesize the phosphorothioate under the promotion of a chlorate agent 1,3-dichloro-5,5-dimethylhydan
