42847-71-2Relevant articles and documents
EINIGE NEUE THIOPHOSPHINSAEUREAMIDE R2P(S)NHR': SYNTHESE UND KERNRESONANZSPEKTROSKOPISCHE UNTERSUCHUNGEN
Kuchen, W.,Langsch, D.,Peters, W.
, p. 55 - 61 (2007/10/02)
P,P-Dialkylthiophosphinic acid amides R2P(S)HNR' (R=Me, iPr, tBu; R'=Me, Et, iPr, cHex, tBu, Ph, etc.) have been obtained by reaction of the corresponding aminophosphines with sulfur or by reaction of dimethylthiophosphorylhalides with primary amines.Their 31P- and 13C-NMR spectra are discussed.The di-t-butylthiophosphinic compounds proved to be remarkably stable against moisture and oxygen.