443906-41-0Relevant academic research and scientific papers
Synthesis of model molecules and NMR analysis of polymeric reagents based on propane-1,3-dithiol and 1,3-dithiane systems
Lucchesini, Francesco,Bertini, Vincenzo,Pocci, Marco,Micali, Eugenio,De Munno, Angela
, p. 1546 - 1550 (2007/10/03)
Purposely synthesized model compounds, one- and two-dimensional NMR spectra and simulations are used for a full 1H and 13C NMR spectroscopic investigation of soluble copolymeric reagents for supported organic syntheses containing (1,3-propanediyl)bis(benzenesulfonate), (1,3-propanediyl)bis(thioacetate), propane-1,3-dithiol, and 1,3-dithiane functions. The collected NMR spectroscopic data confirm the possibility of rapid and accurate assessments of preparations and applications of the newly prepared copolymeric reagents, without resorting to special equipment.
