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Benzeneethanimidoyl chloride, N-hydroxy-α-phenyl-, also known as N-hydroxy-α-phenylbenzeneacetoimidate, is an organic compound with the chemical formula C13H10ClNO2. It is a derivative of benzeneacetoimidate, featuring a hydroxyl group attached to the α-carbon and a phenyl group on the nitrogen atom. Benzeneethanimidoyl chloride, N-hydroxy-a-phenyl- is a valuable intermediate in the synthesis of various pharmaceuticals, agrochemicals, and other specialty chemicals due to its unique reactivity and functional group versatility. It is commonly used in the preparation of amides, esters, and other nitrogen-containing compounds through nucleophilic substitution reactions. The compound is typically synthesized through the reaction of α-phenylbenzeneacetoimidate with a suitable oxidizing agent, such as hydrogen peroxide or sodium hypochlorite, to introduce the hydroxyl group. It is important to handle Benzeneethanimidoyl chloride, N-hydroxy-a-phenyl- with care, as it is sensitive to moisture and can undergo side reactions, and it is also considered to be a hazardous substance due to its potential toxicity and reactivity.

4467-90-7

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4467-90-7 Usage

Check Digit Verification of cas no

The CAS Registry Mumber 4467-90-7 includes 7 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 4 digits, 4,4,6 and 7 respectively; the second part has 2 digits, 9 and 0 respectively.
Calculate Digit Verification of CAS Registry Number 4467-90:
(6*4)+(5*4)+(4*6)+(3*7)+(2*9)+(1*0)=107
107 % 10 = 7
So 4467-90-7 is a valid CAS Registry Number.

4467-90-7Relevant academic research and scientific papers

An efficient method for the synthesis of α-arylated nitroalkanes and α-arylated hydroximoyl chlorides mediated by AlCl3

Tu, Zhijay,Rama Raju,Liou, Tzuo-Rung,Kavala, Veerababurao,Kuo, Chun-Wei,Jang, Yaochung,Shih, Yu-Hsuan,Wang, Chun-Chao,Yao, Ching-Fa

experimental part, p. 2436 - 2442 (2009/07/25)

Friedel-Crafts alkylation of various arenes/heteroarenes to β-nitrostyrenes mediated by aluminum chloride is described. The interesting feature of this methodology pertain the formation of different products by tuning the reaction temperature. α-Arylated

Synthesis of isoxazole conjugates of 1,4-benzodioxane moiety via intermolecular 1,3-dipolar cycloaddition

Vaidya, Vipraja V.,Wankhede, Karuna S.,Nara, Susheel J.,Salunkhe, Manikrao M.,Trivedi, Girish K.

body text, p. 3856 - 3866 (2009/12/08)

1,3-Dipolar cycloaddition was utilized as a tool to conjugate the 1,4-benzodioxane moiety with several biologically active compounds such as steroid, sugar, and other aromatic scaffolds via isoxazole or triazole bridge. The propynyl ether of 2-hydroxymethyl-1,4-benzodioxane underwent 1,3-dipolar cycloadditions smoothly with different in situ generated nitrile oxides in good yields. The triazole conjugate of 1,4-benzodioxane was synthesized via click chemistry. Copyright Taylor & Francis Group, LLC.

A facile one-pot preparation of isothiocyanates from aldoximes

Kim, Jae Nyoung,Jung, Keum Shin,Lee, Hong Jung,Son, Ji Suk

, p. 1597 - 1598 (2007/10/03)

Isothiocyanates 2a-l were prepared in excellent yields in a one-pot reaction from aldoxime derivatives 1a-l by successive treatment of aldoxime with N-chlorosuccinimide (NCS), thiourea, and triethylamine. The use of HCl/DMF/Oxone system in the reaction instead of NCS was equally effective.

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