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54-91-1

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54-91-1 Usage

Originator

Vercyte ,Abbott ,US ,1966

Manufacturing Process

To a solution of 17.2 g (0.10 mol) of 3-bromopropionyl chloride in 100 ml of anhydrous benzene was added dropwise with stirring a solution of 8.6 g (0.10 mol) of anhydrous piperazine in 20 ml of dry chloroform over a period of 30 minutes. The temperature rose spontaneously to 45°C during the addition. After the temperature ceased to rise, stirring was continued for another hour. The reaction mixture was then filtered to remove the piperazine hydrochloride by-product. The filtrate was evaporated to dryness and the residue recrystallized from ethanol to obtain the desired N,N'-bis-(3bromopropionyl)piperazine as a white crystalline solid melting at 103°C to 104°C. The identity of the product was further established by elemental analysis.

Brand name

Vercyte (Abbott).

Therapeutic Function

Antineoplastic

Safety Profile

Poison by ingestion,subcutaneous and intraperitoneal routes. An experimentalteratogen. Other experimental reproductive effects.Human mutation data reported. When heated todecomposition it emits very toxic fumes of Br- and NOx.

Check Digit Verification of cas no

The CAS Registry Mumber 54-91-1 includes 5 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 2 digits, 5 and 4 respectively; the second part has 2 digits, 9 and 1 respectively.
Calculate Digit Verification of CAS Registry Number 54-91:
(4*5)+(3*4)+(2*9)+(1*1)=51
51 % 10 = 1
So 54-91-1 is a valid CAS Registry Number.
InChI:InChI=1/C10H16Br2N2O2/c11-3-1-9(15)13-5-7-14(8-6-13)10(16)2-4-12/h1-8H2

54-91-1SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 17, 2017

Revision Date: Aug 17, 2017

1.Identification

1.1 GHS Product identifier

Product name 1,1'-(Piperazine-1,4-diyl)bis(3-bromopropan-1-one)

1.2 Other means of identification

Product number -
Other names Pipobroman

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:54-91-1 SDS

54-91-1Downstream Products

54-91-1Relevant articles and documents

Photocatalytic synthesis method of bromopropylpiperazine compound

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Paragraph 006; 0029; 0035-0036; 0039; 0045; 0048; 0054; ..., (2022/03/16)

The invention discloses a photocatalytic synthesis method of a bromopropyl piperazine compound, which is characterized in that bromopropyl alcohol and piperazine are used as raw materials, and the bromopropyl piperazine compound is prepared through photocatalytic reaction in the presence of an oxygen-containing atmosphere, an organic solvent, alkali and a transition metal oxide/C3N4 composite photocatalyst. The bromopropyl alcohol is used as the raw material, SOCl2 is avoided, and the bromopropyl piperazine compound is prepared in a green and economical manner.

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