54815-22-4Relevant academic research and scientific papers
Reactions of diorganyl disulfides with dihaloalkanes in basic reductive media. Synthesis of bis(organylthio)alkanes
Alekminskaya,Russavskaya,Korchevin,Deryagina
, p. 75 - 78 (2007/10/03)
A convenient preparative synthesis of bis(organylthio)alkanes was developed. It is based on alkylation with dihaloalkanes of solutions of diorganyl disulfides in the basic reductive system hydrazine hydrate-alkali. The generation of organylthiolate anions
Synthesis of α-Halogeno-ω-alkylthioalkanes and α,ω-Bisalkylthioalkanes
Anklam, Elke
, p. 841 - 843 (2007/10/02)
The reaction of α,ω-dihalogenated alkanes with alkylthiolates affords α-halogeno-ω-alkylthioalkanes 1 as well as α,ω-bisalkylthioalkanes 2.Products 1 (40 examples) and 2 (22 examples) are easily isolated in good yields by flash chromato
