55990-91-5Relevant articles and documents
Synthesis method of substituted thiophenol (by machine translation)
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Paragraph 0017; 0036; 0038; 0039, (2020/06/09)
The invention provides a method for synthesizing substituted thiophenol, which comprises the following steps of preparing compound V compound and NaHSO3 Or KHHSO3 Reaction synthesis IV compound, compound of formula IV and SO2 Reaction-synthesis III compounds of formula III are passed NaBH in NaOH solution. 4 Of formula II is reduced and the compound of formula II is acidified to give a compound of formula I. The method for synthesizing the substituted thiophenol has the advantages of greenness, high efficiency, easiness in industrial application and the like. (by machine translation)
A useful sulfur-transfer reaction with tetrathiomolybdate: Conversion of arylamines to aryl disulfides
Bhar,Chandrasekaran
, p. 785 - 786 (2007/10/02)
A convenient method for the synthesis of a series of symmetrical aryl disulfides from arylamines via the reaction of their stable diazonium salts with tetrathiomolybdate under anhydrous conditions is described.