56345-01-8Relevant articles and documents
Preparation method of E-2-cyclopentadecenone
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Paragraph 0018; 0026-0038, (2017/08/31)
The invention provides a novel method for synthesizing E-2-cyclopentadecenone by utilizing 2-hydroxy-cyclopentadecanone. The 2-hydroxycyclopentadecanone, metal oxide, concentrated sulfuric acid or concentrated phosphoric acid are added into a non-polar organic solvent and are subjected to elimination reaction to obtain the E-2-cyclopentadecenone. In the reaction, a catalytic amount of the metal oxide is added so that a condition that the elimination reaction cannot be realized through the concentrated sulfuric acid before becomes possible; the raw materials in the novel method are relatively cheap; reaction conditions are moderate, the operation is simple and the production cost is reduced so that the novel method is very suitable for industrialized production.