5707-08-4Relevant academic research and scientific papers
Free radical reaction of dialkyl phosphites and organic dichalcogenides: A new facile and convenient preparation of arylselenophosphates
Xu, Qing,Liang, Chun-Gen,Huang, Xian
, p. 2777 - 2785 (2003)
Azobisisobutyronitrile-initiated free radical reaction of dialkyl phosphites with diaryl diselenides afforded arylselenophosphates in high yields. Arylthiophosphates and aryltellurophosphates can also be synthesized by similar reaction of diaryl disulfide
Accelerating Electrochemical Synthesis through Automated Flow: Efficient Synthesis of Chalcogenophosphites
Amri, Nasser,Wirth, Thomas
supporting information, p. 1894 - 1898 (2020/11/24)
Integrated electrochemical reactors in automated flow systems have been utilised for chalcogenophosphite formations. Multiple electrochemical reactions can be performed using a programmed sequence in a fully autonomous way. Differently functionalised chal
Electrochemical selenation of phosphonates and phosphine oxides
Guo, Shengmei,Li, Sen,Zhang, Zhebin,Yan, Wenjie,Cai, Hu
supporting information, (2020/01/11)
An environmentally friendly electrocatalytic strategy for the synthesis of organoselenophospho-rus between phosphonates /phosphine oxides and selenols/diselenides is reported. The reaction was performed with metal-, base- and oxidant-free at room temperat
Fast and transition metal-free general method for the preparation of chalcogenophosphates
Wang, Junxing,Wang, Xiaolong,Li, Hongjie,Yan, Jie
, p. 75 - 79 (2018/02/14)
In the presence of Cs2CO3 and I2, the coupling reaction of dialkyl phosphites with dichalcogenides (S, Se and Te) proceeds efficiently and completes in several minutes under mild conditions, affording the corresponding cha
Atom-economical selenation of electron-rich arenes and phosphonates with molecular oxygen at room temperature
Bhunia, Samir Kumar,Das, Pritha,Jana, Ranjan
supporting information, p. 9243 - 9250 (2019/01/03)
Organoselenium and selenophosphorus compounds are ubiquitously found in biologically active compounds, agrochemicals, functionalized materials etc. Although selenium is a micronutrient and an essential trace element, its contamination/consumption in highe
Calix[4]arene-assisted KOH-catalyzed synthesis of O,O-dialkyl-Se-aryl phosphoroselenoates
Chen, Sihai,Chen, Jinyang,Xu, Xinhua,He, Yunhua,Yi, Rongnan,Qiu, Renhua
, p. 123 - 127 (2016/07/06)
A convenient and efficient method for the synthesis of O,O-dialkyl-Se-aryl phosphoroselenoates is described via a one pot reaction of diaryl diselenide and O,O-dialkylphosphonate catalyzed by KOH assisted by a co-catalyst of calix[4]arene 3. The calix[4]a
Environmentally benign synthesis and antimicrobial study of novel chalcogenophosphates
Mitra, Shubhanjan,Mukherjee, Sayani,Sen, Sukanta K.,Hajra, Alakananda
supporting information, p. 2198 - 2201 (2014/05/06)
We report in this work an environmentally benign zinc mediated synthesis of aryl and benzyl phosphorochalcogenoates in ethanol within a short reaction time. In vitro antimicrobial study along with statistical analysis and seed germination assay were perfo
Hypervalent iodine in synthesis. 49. A new effective synthesis of Se-phenyl O,O-dialkyl phosphoroselenoates with polymer-supported phenyliodine diacetate
Chen,Chen
, p. 421 - 424 (2007/10/03)
Se-phenyl O,O-dialkyl phosphoroselenoates have been prepared by the one-pot reaction of sodium O,O-dialkyl phosphorates, diphenyl diselenide, and polymer-supported phenyliodine diacetate (PPID).
Hypervalent iodine in synthesis 51: A facile novel synthetic access to Se-phenyl O,O-dialkyl phosphoroselenoates
Chen,Chen
, p. 370 - 371 (2007/10/03)
O,O-Dialkyl phosphorous acids react at room temperature with phenyliodine diacetate (PID), sodium azide and diphenyl diselenide, to afford Se-phenyl O,O-dialkyl phosphoroselenoates in good yields.
