57198-66-0Relevant academic research and scientific papers
CONVERSION OF CYCLIC TRITHIOCARBONATES TO THIOACETALS, INCLUDING 1,3-DITHIANE, BY REDUCTION WITH DIISOBUTYLALUMINIUM HYDRIDE (DIBAL)
Jordis, Ulrich,Rudolf, Manfred
, p. 279 - 284 (2007/10/02)
Cyclic trithiocarbonates can be desulfurized with diisobutylaluminium hydride (DIBAL) to form the corresponding thioacetals.This new synthetic pathway was exploited for the preparation of several Umpolung reagents, including 1,3-dithiane.An efficient isolation of sodium trithocarbonate is described.
