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580-17-6

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580-17-6 Usage

Uses

3-Aminoquinoline was used:in liquid matrix for matrix-assisted laser desorption/ionization mass spectrometry (MALDI-MS) for glycopeptides, carbohydrates and phosphopeptidesin liquid matrix during novel glycan-labeling method for quantitative profiling of N-glycan by MALDI-MS analysisas derivatizing reagent for MALDI-MS analysis of oligosachharides

Safety Profile

Poison by intraperitoneal andintravenous route. Mutation data reported. When heatedto decomposition it emits toxic vapors of NOx.

Purification Methods

It crystallises from *C6H6, toluene, hexane and aqueous EtOH. [Beilstein 22 III/IV 4605, 22/10 V 233.]

Check Digit Verification of cas no

The CAS Registry Mumber 580-17-6 includes 6 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 3 digits, 5,8 and 0 respectively; the second part has 2 digits, 1 and 7 respectively.
Calculate Digit Verification of CAS Registry Number 580-17:
(5*5)+(4*8)+(3*0)+(2*1)+(1*7)=66
66 % 10 = 6
So 580-17-6 is a valid CAS Registry Number.
InChI:InChI=1/C9H8N2/c10-8-5-7-3-1-2-4-9(7)11-6-8/h1-6H,10H2

580-17-6 Well-known Company Product Price

  • Brand
  • (Code)Product description
  • CAS number
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  • Detail
  • Alfa Aesar

  • (A16592)  3-Aminoquinoline, 98%   

  • 580-17-6

  • 1g

  • 215.0CNY

  • Detail
  • Alfa Aesar

  • (A16592)  3-Aminoquinoline, 98%   

  • 580-17-6

  • 5g

  • 744.0CNY

  • Detail
  • Alfa Aesar

  • (A16592)  3-Aminoquinoline, 98%   

  • 580-17-6

  • 25g

  • 3148.0CNY

  • Detail
  • Fluka

  • (07336)  3-Aminoquinoline  matrix substance for MALDI-MS, ≥99.0% (GC)

  • 580-17-6

  • 07336-1G

  • 938.34CNY

  • Detail
  • Aldrich

  • (232289)  3-Aminoquinoline  98%

  • 580-17-6

  • 232289-5G

  • 801.45CNY

  • Detail

580-17-6SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name 3-Aminoquinoline

1.2 Other means of identification

Product number -
Other names 3-Quinolinamine

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:580-17-6 SDS

580-17-6Relevant articles and documents

Unlocking Amides through Selective C–N Bond Cleavage: Allyl Bromide-Mediated Divergent Synthesis of Nitrogen-Containing Functional Groups

Govindan, Karthick,Chen, Nian-Qi,Chuang, Yu-Wei,Lin, Wei-Yu

supporting information, p. 9419 - 9424 (2021/11/30)

We report a new set of reactions based on the unlocking of amides through simple treatment with allyl bromide, creating a common platform for accessing a diverse range of nitrogen-containing functional groups such as primary amides, sulfonamides, primary amines, N-acyl compounds (esters, thioesters, amides), and N-sulfonyl esters. The method has potential industrial applicability, as demonstrated through gram-scale syntheses in batch and in a continuous flow system.

Simple Nickel Salts for the Amination of (Hetero)aryl Bromides and Iodides with Lithium Bis(trimethylsilyl)amide

Martinez, Gabriel Espinosa,Nugent, Joseph W.,Fout, Alison R.

supporting information, p. 2941 - 2944 (2018/09/21)

Recent developments in the chemistry of C-N bond formation and the synthesis of anilines have allowed for the use of first-row transition metals to catalyze these transformations. Much of the progress in this area has been driven by comprehensive screening for privileged/tailored ligands, which can be costly and not readily available in a research laboratory setting. In this communication we report a protocol in which simple nickel salts catalyze the C-N cross-coupling reaction between (hetero)aryl bromides and iodides with lithium bis(trimethylsilyl)amide without the need for any additive ligand. This method is amenable to low nickel catalyst loadings (1%) as well as gram-scale reactions. Because of the good functional group tolerance and compatibility with heterocyclic moieties, this method is useful for academic laboratory settings where access to tailored ligands and noble-metal catalysts could be challenging.

AMINATION AND HYDROXYLATION OF ARYLMETAL COMPOUNDS

-

Paragraph 0257, (2018/03/25)

In one aspect, the present disclosure provides methods of preparing a primary or secondary amine and hydroxylated aromatic compounds. In some embodiments, the aromatic compound may be unsubstituted, substituted, or contain one or more heteroatoms within the rings of the aromatic compound. The methods described herein may be carried out without the need for transition metal catalysts or harsh reaction conditions.

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