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Cupric acetate monohydrate
Cas No: 6046-93-1
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High purity Copper(II) acetate monohydrate CAS:6046-93-1
Cas No: 6046-93-1
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Amadis Chemical offer CAS#6046-93-1;CAT#A832740
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Cupric acetate monohydrate
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COPPER(+2)ACETATE MONOHYDRATE CAS NO.:6046-93-1
Cas No: 6046-93-1
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Cupric acetate monohydrate 6046-93-1
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Cupric Acetate Monohydrate CAS 6046-93-1
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Acetic acid, copper(2+)salt, monohydrate (8CI,9CI) 6046-93-1
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Cupric acetate monohydrate
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6046-93-1 Usage

Preparation

Copper(II) acetate is prepared by treatment of copper(II) oxide, CuO, or copper(II) carbonate, CuCO3, with acetic acid, followed by crystallization:
CuO + 2CH3COOH → (CH3COO)2Cu + H2O

Uses

Used in preparation of Fehling's reagent for sugars

Physical Properties

Bluish-green fine powder; hygroscopic. The monohydrate is dimeric; density 1.88 g/cm3; melts at 115°C; decomposes at 240°C; soluble in water and ethanol; and slightly soluble in ether.

Uses

Copper(II) acetate is used as a pigment for ceramics; in the manufacture of Paris green; in textile dyeing; as a fungicide; and as a catalyst.

Chemical Properties

Dark green small crystal with odour of acetic acid

Purification Methods

Recystallise it twice from warm dilute acetic acid solutions (5mL/g) by cooling. [Beilstein 2 IV 111.]

Toxicity

Copper(II) acetate is moderately toxic by ingestion and possibly other routes of administration.
LD50 oral (rat): c. 600 mg/kg
InChI:InChI=1/C2H4O2.Cu.H2O/c1-2(3)4;;/h1H3,(H,3,4);;1H2/q;+2;/p-1

6046-93-1 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Aldrich (229601)  Copper(II)acetatemonohydrate  99.99% trace metals basis 6046-93-1 229601-50G 7,447.05CNY Detail
Aldrich (229601)  Copper(II)acetatemonohydrate  99.99% trace metals basis 6046-93-1 229601-10G 1,953.90CNY Detail
Sigma-Aldrich (61148)  Copper(II)acetatemonohydrate  puriss. p.a., ≥99.0% (RT) 6046-93-1 61148-500G 2,784.60CNY Detail
Sigma-Aldrich (61148)  Copper(II)acetatemonohydrate  puriss. p.a., ≥99.0% (RT) 6046-93-1 61148-100G 718.38CNY Detail
Sigma-Aldrich (217557)  Copper(II)acetatemonohydrate  ACS reagent, ≥98% 6046-93-1 217557-2.5KG 5,506.02CNY Detail
Sigma-Aldrich (217557)  Copper(II)acetatemonohydrate  ACS reagent, ≥98% 6046-93-1 217557-500G 2,108.34CNY Detail
Sigma-Aldrich (217557)  Copper(II)acetatemonohydrate  ACS reagent, ≥98% 6046-93-1 217557-100G 565.11CNY Detail
Sigma-Aldrich (25038)  Copper(II)acetatemonohydrate  ≥99% (iodometric) 6046-93-1 25038-6X1KG-R 6,657.30CNY Detail
Sigma-Aldrich (25038)  Copper(II)acetatemonohydrate  ≥99% (iodometric) 6046-93-1 25038-500G-R 841.23CNY Detail
Alfa Aesar (14177)  Copper(II) acetate monohydrate, ACS, 98.0-102.0%    6046-93-1 2kg 2508.0CNY Detail
Alfa Aesar (14177)  Copper(II) acetate monohydrate, ACS, 98.0-102.0%    6046-93-1 500g 958.0CNY Detail
Alfa Aesar (14177)  Copper(II) acetate monohydrate, ACS, 98.0-102.0%    6046-93-1 100g 391.0CNY Detail

6046-93-1SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name Copper(II) acetate monohydrate

1.2 Other means of identification

Product number -
Other names copper,diacetate,hydrate

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:6046-93-1 SDS

6046-93-1Synthetic route

Conditions
ConditionsYield
In not given Electrolysis; 20% sodium acetate soln.; Cu anode;;96.3%
In not given Electrolysis; 20% sodium acetate soln.; Cu electrodes; 2-8V; 50-100°C;;
In not given Electrolysis; 20% sodium acetate soln.; Cu electrodes; 2-8V; 50-100°C;;
sodium acetate
127-09-3

sodium acetate

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
With acetic acid; sodium chloride Electrolysis;
calcium acetate
62-54-4

calcium acetate

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
With copper(I) sulfate; copper(II) sulfate
acetic acid
64-19-7

acetic acid

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
With basic verdigris
acetic acid
64-19-7

acetic acid

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

acetic acid

acetic acid

copper turnings

copper turnings

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
With air
water

water

copper hydroxide
20427-59-2

copper hydroxide

acetic acid
64-19-7

acetic acid

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In water Cu(OH)2 treated with aq. soln. of acetic acid;
acetic acid
64-19-7

acetic acid

copper(II) oxide

copper(II) oxide

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In acetic acid 2h; excess of concd. acetic acid;;
In acetic acid 2h; excess of concd. acetic acid;;
ethyl acetate
141-78-6

ethyl acetate

copper(II) oxide

copper(II) oxide

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
in the warm;;
in the warm;;
copper(II) nitrate

copper(II) nitrate

acetic acid
64-19-7

acetic acid

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In ammonia concd. acetic acid in excess; concd. aq. NH3; boiling;;
In ammonia aq. ammonia=NH3; concd. acetic acid in excess; concd. aq. NH3; boiling;;
calcium acetate
62-54-4

calcium acetate

copper(II) sulfate
7758-99-8

copper(II) sulfate

acetic acid
64-19-7

acetic acid

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
excess of acetic acid; at 80°C;; evaporation at maximal 66°C or in vacuum;;
excess of acetic acid; at 80°C;; evaporation at maximal 66°C or in vacuum;;
copper diacetate
142-71-2

copper diacetate

acetic acid
64-19-7

acetic acid

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In water density at 15°C <1.10;;
In water density at 15°C <1.10;;
In not given evaporation at 33°C;;
copper(II) sulfate
7758-99-8

copper(II) sulfate

acetic acid
64-19-7

acetic acid

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In ammonia concd. acetic acid in excess; concd. aq. NH3; boiling;;
In ammonia aq. ammonia=NH3; concd. acetic acid in excess; concd. aq. NH3; boiling;;
copper(II) carbonate

copper(II) carbonate

acetic acid
64-19-7

acetic acid

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In acetic acid prepn. from CuCO3 and acetic acid; recrystd. (H2O);
copper hydroxide
20427-59-2

copper hydroxide

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In acetic acid at ambient temp. or at 40-45°C; 8-10% acetic acid;;
In acetic acid
In acetic acid at ambient temp. or at 40-45°C; 8-10% acetic acid;;
In acetic acid
Conditions
ConditionsYield
With air or O2 In not given several h until formation of heat ends;; precipitation with acetic acid;;
With oxygen In not given at 35-40°C treated 2h each with NH4-acetate soln. and O2-containing gas stream;;
With O2 In not given at 35-40°C treated 2h each with NH4-acetate soln. and O2-containing gas stream;;
With air or O2 In not given several h until formation of heat ends;; precipitation with acetic acid;;
calcium acetate
62-54-4

calcium acetate

copper(II) sulfate
7758-99-8

copper(II) sulfate

A

calcium sulfate

calcium sulfate

B

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In not given boiling soln.; Fe-free CuSO4;; precipitation on evaporation;;
In not given boiling soln.; Fe-free CuSO4;; precipitation on evaporation;;
acetic acid ; acidic copper (II)-acetate
71327-10-1

acetic acid ; acidic copper (II)-acetate

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
in moist atmosphere;;
In water evapn. at 50°C;;
in moist atmosphere;;
In water evapn. at 50°C;;
acetic acid ; acidic copper (II)-acetate
71327-10-1

acetic acid ; acidic copper (II)-acetate

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In neat (no solvent) by air moisture in 15 d;;
In neat (no solvent) by air moisture in 15 d;;
calcium copper acetate hexahydrate

calcium copper acetate hexahydrate

A

water
7732-18-5

water

B

calcium acetate hydrate
114460-21-8

calcium acetate hydrate

C

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
at 76.2-78°C at ambient pressure during several hours;;
at 50°C at 6000 atm.;;
at 75°C at 1 atm.;;
[Cu(tris(3,5-dimethylpyrazolyl)methane)(NO2)]

[Cu(tris(3,5-dimethylpyrazolyl)methane)(NO2)]

acetic acid
64-19-7

acetic acid

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In dichloromethane Kinetics; solvent-removed, crystd. (CH2Cl2/Et2O);
(tris(3,5-diethyl-1-pyrazolyl)methane)Cu(NO2)

(tris(3,5-diethyl-1-pyrazolyl)methane)Cu(NO2)

acetic acid
64-19-7

acetic acid

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In dichloromethane Kinetics; solvent-removed, crystd. (CH2Cl2/Et2O);
Conditions
ConditionsYield
In not given Electrolysis; 20% sodium acetate soln.; Cu anode;;96.3%
In not given Electrolysis; 20% sodium acetate soln.; Cu electrodes; 2-8V; 50-100°C;;
In not given Electrolysis; 20% sodium acetate soln.; Cu electrodes; 2-8V; 50-100°C;;
sodium acetate
127-09-3

sodium acetate

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
With acetic acid; sodium chloride Electrolysis;
calcium acetate
62-54-4

calcium acetate

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
With copper(I) sulfate; copper(II) sulfate
acetic acid
64-19-7

acetic acid

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
With basic verdigris
acetic acid
64-19-7

acetic acid

basic copper carbonate

basic copper carbonate

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

acetic acid
64-19-7

acetic acid

copper turnings

copper turnings

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
With air
water
7732-18-5

water

copper hydroxide
20427-59-2

copper hydroxide

acetic acid
64-19-7

acetic acid

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In water Cu(OH)2 treated with aq. soln. of acetic acid;
acetic acid
64-19-7

acetic acid

copper(II) oxide

copper(II) oxide

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In acetic acid 2h; excess of concd. acetic acid;;
In acetic acid 2h; excess of concd. acetic acid;;
ethyl acetate
141-78-6

ethyl acetate

copper(II) oxide

copper(II) oxide

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
in the warm;;
in the warm;;
copper(II) nitrate

copper(II) nitrate

acetic acid
64-19-7

acetic acid

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In ammonia concd. acetic acid in excess; concd. aq. NH3; boiling;;
In ammonia aq. ammonia=NH3; concd. acetic acid in excess; concd. aq. NH3; boiling;;
calcium acetate
62-54-4

calcium acetate

copper(II) sulfate
7758-99-8

copper(II) sulfate

acetic acid
64-19-7

acetic acid

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
excess of acetic acid; at 80°C;; evaporation at maximal 66°C or in vacuum;;
excess of acetic acid; at 80°C;; evaporation at maximal 66°C or in vacuum;;
copper diacetate
142-71-2

copper diacetate

acetic acid
64-19-7

acetic acid

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In water density at 15°C <1.10;;
In water density at 15°C <1.10;;
In not given evaporation at 33°C;;
copper(II) sulfate
7758-99-8

copper(II) sulfate

acetic acid
64-19-7

acetic acid

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In ammonia concd. acetic acid in excess; concd. aq. NH3; boiling;;
In ammonia aq. ammonia=NH3; concd. acetic acid in excess; concd. aq. NH3; boiling;;
copper(II) carbonate

copper(II) carbonate

acetic acid
64-19-7

acetic acid

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In acetic acid prepn. from CuCO3 and acetic acid; recrystd. (H2O);
copper hydroxide
20427-59-2

copper hydroxide

acetic acid
64-19-7

acetic acid

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In acetic acid at ambient temp. or at 40-45°C; 8-10% acetic acid;;
In acetic acid
In acetic acid at ambient temp. or at 40-45°C; 8-10% acetic acid;;
In acetic acid
Conditions
ConditionsYield
With air or O2 In not given several h until formation of heat ends;; precipitation with acetic acid;;
With oxygen In not given at 35-40°C treated 2h each with NH4-acetate soln. and O2-containing gas stream;;
With O2 In not given at 35-40°C treated 2h each with NH4-acetate soln. and O2-containing gas stream;;
With air or O2 In not given several h until formation of heat ends;; precipitation with acetic acid;;
calcium acetate
62-54-4

calcium acetate

copper(II) sulfate
7758-99-8

copper(II) sulfate

A

calcium sulfate

calcium sulfate

B

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In not given boiling soln.; Fe-free CuSO4;; precipitation on evaporation;;
In not given boiling soln.; Fe-free CuSO4;; precipitation on evaporation;;
acetic acid ; acidic copper (II)-acetate
71327-10-1

acetic acid ; acidic copper (II)-acetate

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
in moist atmosphere;;
In water evapn. at 50°C;;
in moist atmosphere;;
In water evapn. at 50°C;;
acetic acid ; acidic copper (II)-acetate
71327-10-1

acetic acid ; acidic copper (II)-acetate

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In neat (no solvent) by air moisture in 15 d;;
In neat (no solvent) by air moisture in 15 d;;
calcium copper acetate hexahydrate

calcium copper acetate hexahydrate

A

water
7732-18-5

water

B

calcium acetate hydrate
114460-21-8

calcium acetate hydrate

C

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
at 76.2-78°C at ambient pressure during several hours;;
at 50°C at 6000 atm.;;
at 75°C at 1 atm.;;
[Cu(tris(3,5-dimethylpyrazolyl)methane)(NO2)]

[Cu(tris(3,5-dimethylpyrazolyl)methane)(NO2)]

acetic acid
64-19-7

acetic acid

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In dichloromethane Kinetics; solvent-removed, crystd. (CH2Cl2/Et2O);
(tris(3,5-diethyl-1-pyrazolyl)methane)Cu(NO2)

(tris(3,5-diethyl-1-pyrazolyl)methane)Cu(NO2)

acetic acid
64-19-7

acetic acid

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In dichloromethane Kinetics; solvent-removed, crystd. (CH2Cl2/Et2O);
(tris(3,5-diisopropyl-1-pyrazolyl)methane)Cu(NO2)

(tris(3,5-diisopropyl-1-pyrazolyl)methane)Cu(NO2)

acetic acid
64-19-7

acetic acid

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In dichloromethane Kinetics; solvent-removed, crystd. (CH2Cl2/Et2O);
C14H23NO4Si

C14H23NO4Si

C28H44CuN2O8Si2

C28H44CuN2O8Si2

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
In methanol for 3h; Reflux;
copper(ll) sulfate pentahydrate

copper(ll) sulfate pentahydrate

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Conditions
ConditionsYield
With sodium citrate; sodium hydroxide; ascorbic acid In water for 2h;
Mo(CO)5((C6H5)2PNHCH2CH2NCHC6H4OH)
102942-30-3

Mo(CO)5((C6H5)2PNHCH2CH2NCHC6H4OH)

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

trans-{Mo(CO)5(Ph2PNHCH2CH2N=CHC6H4-o-O)}2Cu

trans-{Mo(CO)5(Ph2PNHCH2CH2N=CHC6H4-o-O)}2Cu

Conditions
ConditionsYield
In tetrahydrofuran A mixt. of Cu(OAc)2*H2O and Mo(CO)5(Ph2PNHCH2CH2NCHC6H4OH) in THF was stirred under Ar at ambient temp. for 42 h. The color of the mixt. changed from bright yellow to dark green overnight.; The mixt. was filtered and then the filtrate evapd. to dryness to yield {Mo(CO)5(Ph2PNHCH2CH2NCHC6H4O)}2Cu.;100%
{copper(II)-(N,N'-disalicylidene-1,3-propanediamine)}
21051-65-0

{copper(II)-(N,N'-disalicylidene-1,3-propanediamine)}

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

{copper(II)-(N,N'-disalicylidene-1,3-propanediamine-μ-O,O')-(μ-CH3COO)Cu(μ-CH3O)2-Cu(μ-CH3COO)(N,N'-disalicylidene-1,3-propanediamine-μ-O,O')Cu}

{copper(II)-(N,N'-disalicylidene-1,3-propanediamine-μ-O,O')-(μ-CH3COO)Cu(μ-CH3O)2-Cu(μ-CH3COO)(N,N'-disalicylidene-1,3-propanediamine-μ-O,O')Cu}

Conditions
ConditionsYield
With N(C2H5)3; CH3OH In methanol byproducts: CH3COOH; N2 bubbled through Cu(CH3COO)2 soln. for 10 min; addn. of (Cu(salpd)) and N(C2H5)3; stirred at 25°C for 36 h; filtration; washed (MeOH/Et2O); dried at 60°C under reduced pressure for 40 min; elem. anal.; IR;100%
(CO)5Mo(Ph2PNH(CH2)3NCHC6H4-o-OH)
127522-45-6

(CO)5Mo(Ph2PNH(CH2)3NCHC6H4-o-OH)

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

Mo2Cu(2+)*10CO*2(C6H5)2PNH(CH2)3NCHC6H4O(1-)=((CO)5Mo((C6H5)2PNH(CH2)3NCHC6H4O))2Cu

Mo2Cu(2+)*10CO*2(C6H5)2PNH(CH2)3NCHC6H4O(1-)=((CO)5Mo((C6H5)2PNH(CH2)3NCHC6H4O))2Cu

Conditions
ConditionsYield
In tetrahydrofuran react. under N2; stirring a soln. of Mo-complex and Cu-compd. in THF for 4 days at ambient temp.; evapn. to dryness, recrystn. from CH2Cl2/hexane; elem. anal.;100%
5,10,15,20-tetrakis[(3,5-di-tert-butylphenyl)]porphyrin

5,10,15,20-tetrakis[(3,5-di-tert-butylphenyl)]porphyrin

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

[5,10,15,20-tetrakis(3',5'-di-tert-butylphenyl)porphyrinato]copper(II)
146164-93-4

[5,10,15,20-tetrakis(3',5'-di-tert-butylphenyl)porphyrinato]copper(II)

Conditions
ConditionsYield
In methanol; dichloromethane refluxing a mixt. of porphyrine and copper salt in CH2Cl2 and CH3OH for 1.5 h, cooling; evapn., passing through a plug of silica (CH2Cl2), evapn.;100%
ammonium hexafluorophosphate

ammonium hexafluorophosphate

copper(II) acetate monohydrate
6046-93-1

copper(II) acetate monohydrate

4',4''''-bis(methylsulfanyl)-2,2':6',2'':6'',2''':6''',2'''':6'''',2'''''-sexipyridine
147439-49-4

4',4''''-bis(methylsulfanyl)-2,2':6',2'':6'',2''':6''',2'''':6'''',2'''''-sexipyridine

{Cu2((C5H4N)2(C5H2(CH3S)N)2(C5H3N)2)2}(4+)*4PF6(1-)*3H2O={Cu2((C5H4N)2(C5H2(CH3S)N)2(C5H3N)2)2}{PF6}4*3H2O

{Cu2((C5H4N)2(C5H2(CH3S)N)2(C5H3N)2)2}(4+)*4PF6(1-)*3H2O={Cu2((C5H4N)2(C5H2(CH3S)N)2(C5H3N)2)2}{PF6}4*3H2O

Conditions
ConditionsYield
In methanol addn. of 1.79E-4 mol sexipyridine to a soln. of 1.8E-4 mol Cu(O2CCH3)2*H2O in methanol; stirring for 4 h at room temperature; treating with a satd. methanolic soln. of NH4PF6; pptn.;; collection; washing with methanol; recrystallization from CH3CN/diethyl ether; elem. anal.;;100%

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