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6223-35-4

6223-35-4

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  • High Quality Oled CAS 6223-35-4 1-Azulenesulfonic acid,3,8-dimethyl-5-(1-methylethyl)-, sodium salt (1:1)

    Cas No: 6223-35-4

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6223-35-4 Usage

Description

Sodium gualenate is unstable, it will decompose under light, air oxidation and high temperature environment, and it is easy to remove the sulfonic acid group. According to existing reports, it is common for sodium azulene sulfonate to contain half or one crystal water.

Uses

Sodium gualenate is an active ingredient of chamomile flowers, which has strong anti-pepsin, anti-inflammatory, antibacterial, anti-allergic, and promotion of mucosal metabolism. It is mainly used to study duodenal ulcer, gastric ulcer and gastritis.

Mechanism of action

Sodium gualenate inhibits the release of histamine from inflammatory cells through local direct action; increases the synthesis of prostaglandin E2 in the mucosa, promotes granulation formation and epithelial cell regeneration; and can reduce the activity of pepsin.

Check Digit Verification of cas no

The CAS Registry Mumber 6223-35-4 includes 7 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 4 digits, 6,2,2 and 3 respectively; the second part has 2 digits, 3 and 5 respectively.
Calculate Digit Verification of CAS Registry Number 6223-35:
(6*6)+(5*2)+(4*2)+(3*3)+(2*3)+(1*5)=74
74 % 10 = 4
So 6223-35-4 is a valid CAS Registry Number.
InChI:InChI=1/C15H18O3S.Na/c1-9(2)12-6-5-10(3)15-13(8-12)11(4)7-14(15)19(16,17)18;/h5-9H,1-4H3,(H,16,17,18);/q;+1/p-1

6223-35-4 Well-known Company Product Price

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  • TCI America

  • (S0976)  Sodium 7-Isopropyl-1,4-dimethylazulene-3-sulfonate  >98.0%(HPLC)(T)

  • 6223-35-4

  • 1g

  • 1,200.00CNY

  • Detail

  • TCI America

  • (S0976)  Sodium 7-Isopropyl-1,4-dimethylazulene-3-sulfonate  >98.0%(HPLC)(T)

  • 6223-35-4

  • 5g

  • 4,690.00CNY

  • Detail

6223-35-4SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name sodium,3,8-dimethyl-5-propan-2-ylazulene-1-sulfonate

1.2 Other means of identification

Product number -
Other names sodium 5-isopropyl-3,8-dimethylazulene-1-sulfonate

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

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More Details:6223-35-4 SDS

6223-35-4Synthetic route

7-isopropyl-1,4-dimethyl-azulene
489-84-9

7-isopropyl-1,4-dimethyl-azulene

Azulon
6223-35-4

Azulon

Conditions
ConditionsYield
With sulfuric acid; acetic anhydride at 20℃; for 2h; Cooling with ice;87.5%
Stage #1: 7-isopropyl-1,4-dimethyl-azulene With sulfuric acid; acetic anhydride at 20℃; for 4h;
Stage #2: With sodium hydroxide In water		57%
Multi-step reaction with 2 steps
1: sulfuric acid; acetic anhydride / 3 h / 20 °C
2: sodium hydroxide
View Scheme
Stage #1: 7-isopropyl-1,4-dimethyl-azulene With sulfuric acid; acetic anhydride at 20℃; for 3h;
Stage #2: With sodium hydroxide
5-isopropyl-3,8-dimethyl-azulene-1-sulfonic acid
16915-32-5

5-isopropyl-3,8-dimethyl-azulene-1-sulfonic acid

Azulon
6223-35-4

Azulon

Conditions
ConditionsYield
With sodium hydroxide
piperazine
110-85-0

piperazine

Azulon
6223-35-4

Azulon

1-((5-isopropyl-3,8-dimethylazulen-1-yl)sulfonyl)piperazine

1-((5-isopropyl-3,8-dimethylazulen-1-yl)sulfonyl)piperazine

Conditions
ConditionsYield
Stage #1: Azulon With pyridine; oxalyl dichloride In dichloromethane
Stage #2: piperazine With pyridine; triethylamine		43%
Azulon
6223-35-4

Azulon

N-ethyl-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide
1338350-96-1

N-ethyl-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / Cooling with ice
2: pyridine; triethylamine / dichloromethane / 1 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide; pyridine; oxalyl dichloride / dichloromethane / Cooling with ice
2: triethylamine; pyridine / dichloromethane / 1 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

N-cyclohexyl-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide
1338350-97-2

N-cyclohexyl-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / Cooling with ice
2: pyridine; triethylamine / dichloromethane / 1 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide; pyridine; oxalyl dichloride / dichloromethane / Cooling with ice
2: triethylamine; pyridine / dichloromethane / 1 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

N-benzyl-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide
1338350-98-3

N-benzyl-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / Cooling with ice
2: pyridine; triethylamine / dichloromethane / 1 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide; pyridine; oxalyl dichloride / dichloromethane / Cooling with ice
2: triethylamine; pyridine / dichloromethane / 1 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

N-(4-chlorophenyl)-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide
1338350-99-4

N-(4-chlorophenyl)-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / Cooling with ice
2: pyridine; triethylamine / dichloromethane / 1 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide; pyridine; oxalyl dichloride / dichloromethane / Cooling with ice
2: triethylamine; pyridine / dichloromethane / 1 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

N-(4-aminophenyl)-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide
1338351-00-0

N-(4-aminophenyl)-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / Cooling with ice
2: pyridine; triethylamine / dichloromethane / 1 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide; pyridine; oxalyl dichloride / dichloromethane / Cooling with ice
2: triethylamine; pyridine / dichloromethane / 1 h / 20 °C
View Scheme
Multi-step reaction with 3 steps
1: thionyl chloride / dichloromethane / 4 h / 0 °C
2: dichloromethane / 12 h
3: trifluoroacetic acid / dichloromethane / 3 h
View Scheme
Azulon
6223-35-4

Azulon

N-[4-(benzylideneamino)phenyl]-5-isopropyl-3,8-dimethylazulene-1-sulfonamide
1338351-02-2

N-[4-(benzylideneamino)phenyl]-5-isopropyl-3,8-dimethylazulene-1-sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: pyridine; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / Cooling with ice
2: pyridine; triethylamine / dichloromethane / 1 h / 20 °C
3: ethanol / 1 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

N-[4-(2-hydroxybenzylideneamino)phenyl]-5-isopropyl-3,8-dimethylazulene-1-sulfonamide
1338351-03-3

N-[4-(2-hydroxybenzylideneamino)phenyl]-5-isopropyl-3,8-dimethylazulene-1-sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: pyridine; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / Cooling with ice
2: pyridine; triethylamine / dichloromethane / 1 h / 20 °C
3: ethanol / 1 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

N-[4-(2-thienylmethyleneamino)phenyl]-5-isopropyl-3,8-dimethylazulene-1-sulfonamide
1338351-04-4

N-[4-(2-thienylmethyleneamino)phenyl]-5-isopropyl-3,8-dimethylazulene-1-sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: pyridine; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / Cooling with ice
2: pyridine; triethylamine / dichloromethane / 1 h / 20 °C
3: ethanol / 1 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

N-amino-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide
1338351-09-9

N-amino-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / Cooling with ice
2: pyridine; triethylamine; hydrazine
View Scheme
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide; pyridine; oxalyl dichloride / dichloromethane / Cooling with ice
2: triethylamine; hydrazine hydrate; pyridine / dichloromethane / 1 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

N'-(4-methoxybenzylidene)-5-isopropyl-3,8-dimethylazulene-1-sulfonohydrazide
1338351-05-5

N'-(4-methoxybenzylidene)-5-isopropyl-3,8-dimethylazulene-1-sulfonohydrazide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: pyridine; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / Cooling with ice
2: pyridine; triethylamine; hydrazine
3: ethanol / 1 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

N'-(4-trifluoromethylbenzylidene)-5-isopropyl-3,8-dimethylazulene-1-sulfonohydrazide
1338351-06-6

N'-(4-trifluoromethylbenzylidene)-5-isopropyl-3,8-dimethylazulene-1-sulfonohydrazide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: pyridine; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / Cooling with ice
2: pyridine; triethylamine; hydrazine
3: ethanol / 1 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

N'-(2-hydroxybenzylidene)-5-isopropyl-3,8-dimethylazulene-1-sulfonohydrazide
1338351-07-7

N'-(2-hydroxybenzylidene)-5-isopropyl-3,8-dimethylazulene-1-sulfonohydrazide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: pyridine; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / Cooling with ice
2: pyridine; triethylamine; hydrazine
3: ethanol / 1 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

N'-(2-thienylmethylene)-5-isopropyl-3,8-dimethylazulene-1-sulfonohydrazide
1338351-08-8

N'-(2-thienylmethylene)-5-isopropyl-3,8-dimethylazulene-1-sulfonohydrazide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: pyridine; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / Cooling with ice
2: pyridine; triethylamine; hydrazine
3: ethanol / 1 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

N-(3-bromophenyl)-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide
1338350-89-2

N-(3-bromophenyl)-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / Cooling with ice
2: pyridine; triethylamine / dichloromethane / 1 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide; pyridine; oxalyl dichloride / dichloromethane / Cooling with ice
2: triethylamine; pyridine / dichloromethane / 1 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

N-(2,4-dimethoxyphenyl)-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide
1338350-90-5

N-(2,4-dimethoxyphenyl)-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / Cooling with ice
2: pyridine; triethylamine / dichloromethane / 1 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide; pyridine; oxalyl dichloride / dichloromethane / Cooling with ice
2: triethylamine; pyridine / dichloromethane / 1 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

N,5-diisopropyl-3,8-dimethyl-1-azulene sulfonamide
1338350-91-6

N,5-diisopropyl-3,8-dimethyl-1-azulene sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / Cooling with ice
2: pyridine; triethylamine / dichloromethane / 1 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 0.17 h / 0 °C
2: sodium carbonate decahydrate / 2.5 h / 5 °C
View Scheme
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide; pyridine; oxalyl dichloride / dichloromethane / Cooling with ice
2: triethylamine; pyridine / dichloromethane / 1 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

N-(naphthalen-1-yl)-5-isopropyl-3,8-dimethylazulene-1-sulfonamide
1338350-92-7

N-(naphthalen-1-yl)-5-isopropyl-3,8-dimethylazulene-1-sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / Cooling with ice
2: pyridine; triethylamine / dichloromethane / 1 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide; pyridine; oxalyl dichloride / dichloromethane / Cooling with ice
2: triethylamine; pyridine / dichloromethane / 1 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

N-isobutyl-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide
1338350-93-8

N-isobutyl-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / Cooling with ice
2: pyridine; triethylamine / dichloromethane / 1 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide; pyridine; oxalyl dichloride / dichloromethane / Cooling with ice
2: triethylamine; pyridine / dichloromethane / 1 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

N-propyl-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide
1338350-94-9

N-propyl-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / Cooling with ice
2: pyridine; triethylamine / dichloromethane / 1 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 0.17 h / 0 °C
2: sodium carbonate decahydrate / 1.5 h / 5 °C
View Scheme
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide; pyridine; oxalyl dichloride / dichloromethane / Cooling with ice
2: triethylamine; pyridine / dichloromethane / 1 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

N-(4-methylphenyl)-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide
1338350-95-0

N-(4-methylphenyl)-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / Cooling with ice
2: pyridine; triethylamine / dichloromethane / 1 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide; pyridine; oxalyl dichloride / dichloromethane / Cooling with ice
2: triethylamine; pyridine / dichloromethane / 1 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

5-isopropyl-3,8-dimethyl-azulene-1-sulfonyl chloride
69174-69-2

5-isopropyl-3,8-dimethyl-azulene-1-sulfonyl chloride

Conditions
ConditionsYield
With pyridine; oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane for 0.166667h; Cooling with ice;
With oxalyl dichloride In dichloromethane; N,N-dimethyl-formamide at 0℃; for 0.166667h;
With pyridine; oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane Cooling with ice;
With thionyl chloride In dichloromethane at 0℃; for 4h;
Azulon
6223-35-4

Azulon

C22H24O3S
1436872-40-0

C22H24O3S

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 0.17 h / 0 °C
2: pyridine / N,N-dimethyl-formamide; dimethyl sulfoxide / 2.5 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

C16H18O4S
1436872-41-1

C16H18O4S

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 0.17 h / 0 °C
2: pyridine / N,N-dimethyl-formamide; dimethyl sulfoxide / 1 h / 20 °C
3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / acetone; water / 1 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

C17H20O4S
1436872-42-2

C17H20O4S

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 0.17 h / 0 °C
2: pyridine / N,N-dimethyl-formamide; dimethyl sulfoxide / 2 h / 20 °C
3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / acetone; water / 2 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

C18H22O4S
1436872-43-3

C18H22O4S

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 0.17 h / 0 °C
2: pyridine / N,N-dimethyl-formamide; dimethyl sulfoxide / 2.5 h / 20 °C
3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / acetone; water / 2.5 h / 20 °C
View Scheme
Azulon
6223-35-4

Azulon

C23H28O5S
1436872-44-4

C23H28O5S

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 0.17 h / 0 °C
2: pyridine / N,N-dimethyl-formamide; dimethyl sulfoxide / 2.5 h / 20 °C
3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / acetone; water / 2.5 h / 20 °C
4: ytterbium(III) triflate; acetic anhydride / nitromethane / 18 h / 20 °C
View Scheme

6223-35-4Relevant articles and documents

Synthesis and Biological Evaluation of 3, 8-dimethyl-5-isopropylazulene Derivatives as Anti-gastric Ulcer Agent

Cao, Tingting,Li, Yong,Yang, Ziyao,Yuan, Mingxing,Li, Ying,Yang, Hongjun,Feng, Yuchuan,Yin, Shufan

, p. 264 - 271 (2016)

Recent studies showed that Guaiazulene (GA) and Sodium guaiazulene sulfonate (GAS-Na) have good anti-gastric ulcer effect. Here, two series of GA derivatives were synthesized and evaluated for their anti-gastric ulcer activity. The data obtained from in vivo testing of these compounds in a rodent ethanol-induced stomach injury model are discussed. Among the tested compounds, A1, A4, and A9 (ulcer index: 1.125 ± 1.246**, 1.714 ± 0.756*, 1.875 ± 1.126*) exhibited better anti-gastric ulcer activity than the positive control Omeprazole (2.005 ± 1.011*). The information got from these studies and the results of 3D-SAR investigation may be useful in the design of novel anti-gastric ulcer agents.

N-SUBSTITUTED ISOPROPYLDIMETHYL AZULENE SULFONAMIDE DERIVATIVES, AND PREPARATION METHOD AND USE THEREOF

-

Paragraph 0108-0110, (2014/08/06)

The present invention provides an N-substituted isopropyldimethyl azulene sulfonamide derivative as represented by formula (I), and preparation method and uses thereof, wherein R1 is an alkyl, cycloalkyl, alkenyl, alkynyl, aryl, heteroaryl, amino, or a substituted alkyl, cycloalkyl, alkenyl, alkynyl, aryl, heteroaryl, and amino. The N-substituted isopropyldimethyl azulene sulfonamide derivative can be used in treating gastric ulcer.

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