63181-18-0Relevant academic research and scientific papers
1α-HYDROXY PREVITAMIN D3 AND ITS SELECTIVE FORMATION FROM 1-KETO PREVITAMIN D3
Vanmaele, L. J.,Clercq, P. J. De,Vandewalle, M.,Halkes, S. J.,Overbeek, W. R. M.
, p. 1179 - 1182 (1984)
An efficient method for the preparation of crystalline 1α-hydroxy previtamin D3 is described.Also the stereoselective reduction of 1-keto previtamin 9 is discussed; it was observed that with aluminium hydride 7 is the most abundant product.This stands in contrast with previously reported LiAlH4 and NaBH4 mediated reductions.
