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64464-07-9

64464-07-9

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64464-07-9 Usage

Chemical Properties

White Solid

Uses

Different sources of media describe the Uses of 64464-07-9 differently. You can refer to the following data:
1. Impurity of Carvedilol synthesis.
2. 2-(2-Methoxyphenoxy)ethylamine Hydrochloride (Carvedilol EP Impurity E; Carvedilol Impurity E; Carvedilol USP E) is an impurity of Carvedilol synthesis.

Check Digit Verification of cas no

The CAS Registry Mumber 64464-07-9 includes 8 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 5 digits, 6,4,4,6 and 4 respectively; the second part has 2 digits, 0 and 7 respectively.
Calculate Digit Verification of CAS Registry Number 64464-07:
(7*6)+(6*4)+(5*4)+(4*6)+(3*4)+(2*0)+(1*7)=129
129 % 10 = 9
So 64464-07-9 is a valid CAS Registry Number.
InChI:InChI=1/C9H13NO2.ClH/c1-11-8-4-2-3-5-9(8)12-7-6-10;/h2-5H,6-7,10H2,1H3;1H

64464-07-9 Well-known Company Product Price

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  • Sigma-Aldrich

  • (40551)  2-(2-Methoxyphenoxy)ethylamine hydrochloride monohydrate  analytical standard, pharmaceutical impurity standard

  • 64464-07-9

  • 40551-50MG

  • 8,897.85CNY

  • Detail

64464-07-9SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name 2-(2-Methoxyphenoxy)Ethylamine Hydrochloride Hydrate

1.2 Other means of identification

Product number -
Other names 2-(2-Methoxyphenoxy)ethylamine hydrochloride

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:64464-07-9 SDS

64464-07-9Synthetic route

carbonic acid 2-chloro-1-chloro-methyl-ethyl ester phenyl ester

carbonic acid 2-chloro-1-chloro-methyl-ethyl ester phenyl ester

2-[(2-methoxy)phenoxy]ethylamine hydrochloride
64464-07-9

2-[(2-methoxy)phenoxy]ethylamine hydrochloride

1,3-dichloro-2-propyl-2-(2-methoxyphenoxy)ethylcarbamate(II)
374779-56-3

1,3-dichloro-2-propyl-2-(2-methoxyphenoxy)ethylcarbamate(II)

Conditions
ConditionsYield
Stage #1: 2-[(2-methoxy)phenoxy]ethylamine hydrochloride With triethylamine In ethanol for 0.0833333h;
Stage #2: carbonic acid 2-chloro-1-chloro-methyl-ethyl ester phenyl ester In ethanol at 20℃;		97%
2-[(2-methoxy)phenoxy]ethylamine hydrochloride
64464-07-9

2-[(2-methoxy)phenoxy]ethylamine hydrochloride

2-(2-methoxy-phenoxy)-ethylamine
1836-62-0

2-(2-methoxy-phenoxy)-ethylamine

Conditions
ConditionsYield
With sodium hydroxide In water at 0℃; pH=12 - 14;97%
2-[(2-methoxy)phenoxy]ethylamine hydrochloride
64464-07-9

2-[(2-methoxy)phenoxy]ethylamine hydrochloride

4-(2,3-epoxypropoxy)carbazole
51997-51-4

4-(2,3-epoxypropoxy)carbazole

carvedilol
72956-09-3

carvedilol

Conditions
ConditionsYield
Stage #1: 2-[(2-methoxy)phenoxy]ethylamine hydrochloride With sodium hydroxide In water at 20℃; pH=9 - 9.5;
Stage #2: 4-(2,3-epoxypropoxy)carbazole In water at 80 - 85℃; for 0.75 - 1h; Product distribution / selectivity;		45.99%
Stage #1: 2-[(2-methoxy)phenoxy]ethylamine hydrochloride With sodium hydroxide In water; isopropyl alcohol at 20℃; pH=9 - 9.5;
Stage #2: 4-(2,3-epoxypropoxy)carbazole In water; isopropyl alcohol for 4 - 5h; Product distribution / selectivity; Heating / reflux;		43.05%
With potassium carbonate In i-Amyl alcohol at 80 - 85℃; for 7h;41%
With calcium carbonate In isopropyl alcohol at 80℃; for 4h;
formaldehyd
50-00-0

formaldehyd

2,2-diphenylcyclopentanone
15324-42-2

2,2-diphenylcyclopentanone

2-[(2-methoxy)phenoxy]ethylamine hydrochloride
64464-07-9

2-[(2-methoxy)phenoxy]ethylamine hydrochloride

5-({[2-(2-methoxyphenoxy)ethyl]amino}methyl)-2,2-diphenylcyclopentan-1-one
1353573-77-9

5-({[2-(2-methoxyphenoxy)ethyl]amino}methyl)-2,2-diphenylcyclopentan-1-one

Conditions
ConditionsYield
In ethanol Reflux;36%
formaldehyd
50-00-0

formaldehyd

inden-1-one
83-33-0

inden-1-one

2-[(2-methoxy)phenoxy]ethylamine hydrochloride
64464-07-9

2-[(2-methoxy)phenoxy]ethylamine hydrochloride

2-{[2-(2-Methoxy-phenoxy)-ethylamino]-methyl}-indan-1-one

2-{[2-(2-Methoxy-phenoxy)-ethylamino]-methyl}-indan-1-one

Conditions
ConditionsYield
In isopropyl alcohol Heating;
formaldehyd
50-00-0

formaldehyd

3,4-dihydronaphthalene-1(2H)-one
529-34-0

3,4-dihydronaphthalene-1(2H)-one

2-[(2-methoxy)phenoxy]ethylamine hydrochloride
64464-07-9

2-[(2-methoxy)phenoxy]ethylamine hydrochloride

2-{[2-(2-Methoxy-phenoxy)-ethylamino]-methyl}-3,4-dihydro-2H-naphthalen-1-one
40077-29-0

2-{[2-(2-Methoxy-phenoxy)-ethylamino]-methyl}-3,4-dihydro-2H-naphthalen-1-one

Conditions
ConditionsYield
In isopropyl alcohol Heating;
Phenyl glycidyl ether
122-60-1

Phenyl glycidyl ether

2-[(2-methoxy)phenoxy]ethylamine hydrochloride
64464-07-9

2-[(2-methoxy)phenoxy]ethylamine hydrochloride

N-<2-(2-Methoxy-phenoxy)-aethyl>-2-hydroxy-3-phenoxy-propylamin
3258-69-3

N-<2-(2-Methoxy-phenoxy)-aethyl>-2-hydroxy-3-phenoxy-propylamin

Conditions
ConditionsYield
With sodium hydroxide In propan-1-ol Heating;
2-[(2-methoxy)phenoxy]ethylamine hydrochloride
64464-07-9

2-[(2-methoxy)phenoxy]ethylamine hydrochloride

2-(2-methoxy-phenoxymethyl)-oxirane
2210-74-4

2-(2-methoxy-phenoxymethyl)-oxirane

1-(2-methoxyphenoxy)-3-[2-(2-methoxyphenoxy)ethylamino]propan-2-ol
3258-68-2

1-(2-methoxyphenoxy)-3-[2-(2-methoxyphenoxy)ethylamino]propan-2-ol

Conditions
ConditionsYield
With sodium hydroxide In propan-1-ol Heating;
2-chloro-6-(5-methyl-1H-pyrazol-3-ylamino)-4-methylnicotinonitrile
914086-10-5

2-chloro-6-(5-methyl-1H-pyrazol-3-ylamino)-4-methylnicotinonitrile

2-[(2-methoxy)phenoxy]ethylamine hydrochloride
64464-07-9

2-[(2-methoxy)phenoxy]ethylamine hydrochloride

2-(2-(2-methoxyphenoxy)ethylamino)-6-(5-methyl-1H-pyrazol-3-ylamino)-4-methylnicotinonitrile

2-(2-(2-methoxyphenoxy)ethylamino)-6-(5-methyl-1H-pyrazol-3-ylamino)-4-methylnicotinonitrile

Conditions
ConditionsYield
With sodium hydrogencarbonate In dimethyl sulfoxide at 100℃; for 27h;
2-[(2-methoxy)phenoxy]ethylamine hydrochloride
64464-07-9

2-[(2-methoxy)phenoxy]ethylamine hydrochloride

5-(((9H-carbazol-4-yl)oxy)methyl)-3-(2-(2-methoxyphenoxy)ethyl)oxazolidin-2-one
180987-80-8

5-(((9H-carbazol-4-yl)oxy)methyl)-3-(2-(2-methoxyphenoxy)ethyl)oxazolidin-2-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: triethylamine / ethanol / 0.08 h
1.2: 20 °C
2.1: sodium hydride / tetrahydrofuran / 1 h / 20 - 67 °C / Nitrogen atmosphere
3.1: potassium carbonate / sodium dithionite; potassium iodide / ethanol / 24 h / Nitrogen atmosphere; Heating / reflux
View Scheme
2-[(2-methoxy)phenoxy]ethylamine hydrochloride
64464-07-9

2-[(2-methoxy)phenoxy]ethylamine hydrochloride

carvedilol
72956-09-3

carvedilol

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: triethylamine / ethanol / 0.08 h
1.2: 20 °C
2.1: sodium hydride / tetrahydrofuran / 1 h / 20 - 67 °C / Nitrogen atmosphere
3.1: potassium carbonate / sodium dithionite; potassium iodide / ethanol / 24 h / Nitrogen atmosphere; Heating / reflux
4.1: sodium hydroxide / ethanol; water / 20 °C / Nitrogen atmosphere
View Scheme

64464-07-9Upstream product

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