65210-10-8Relevant academic research and scientific papers
Microwave-enhanced synthesis of phosphonoacetamides
Gruber, Nadia,Mollo, Mara C.,Zani, Mariana,Orelli, Liliana R.
experimental part, p. 738 - 746 (2011/12/15)
An efficient microwave protocol is described for the Michaelis-Arbuzov synthesis of secondary and tertiary N-aryl (and alkyl) (diethylphosphono) acetamides 1, by reaction of chloro- and bromoacetamides with triethyl phosphite in the presence of catalytic
Horner-Wadsworth-Emmons olefination of nonstabilized phosphonates. A new synthetic approach to β,γ-unsaturated amides
Janecki,Janecki, Tomasz,Bodalski,Bodalski, Ryszard,Wieczorek,Wieczorek, Michakl,Bujacz,Bujacz, Grzegorz
, p. 1721 - 1740 (2007/10/02)
Aminolysis of readily accessible β-diethoxyphosphonyl-γ-butyrolactones 5 and 22 provides a convenient entry to (E)-β,γ-unsaturated amides 8 and 24 respectively. The key step of the aminolysis involves elimination of diethoxyphosporic acid from the corresp
