65833-20-7Relevant academic research and scientific papers
Synthesis and characterization of new compounds containing 1,4-dithiintetracarboxydiimide units
Gǎinǎ, Constantin
, p. 601 - 607 (2007/10/03)
New compounds containing 1,4-dithiintetracarboxydiimide units were synthesized by the disubstitution reaction of N-substituted 2,3- dichloromaleimide with sodium sulflde nonahydrate or thiourea. IR, UV-vis and 1H-NMR spectroscopy, as well as elemental analysis, confirmed their structures. Thermal conversion of 1,4-dithiine ring to thiophene was monitored by differential calorimetry (DSC) and thermogravimetric (TGA) measurements.
