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Electrochemical Deblocking, III. - On the Electrochemical Reduction of β-Haloethyl Diphenylphosphates
Engels, Joachim
, p. 557 - 563 (2007/10/02)
Controlled potential electroreduction of the β-haloethyl diphenylphosphates 3a-e at the mercury cathode yielded diphenylphosphate.The dependence of the reduction potentials on the halogen used and the influence of geminal halogens has been investigated by cyclic voltammetry (Figure 1, Table 1).Preparative electroreduction and its possible by-products depending upon the conditions used in the electrolysis have been analyzed and discussed.
