67560-64-9Relevant academic research and scientific papers
A SYNTHESIS OF (+/-)-PINORESINOL AND ITS RELATED COMPOUND USING POTASSIUM PERSULFATE (K2S2O8) OXIDATION OF BENZOYLACETATES
Maruyama, Jun,Kobayashi, Miho,Miyashita, Masaaki,Kouno, Isao,Irie, Hiroshi
, p. 839 - 846 (2007/10/02)
A synthesis of (+/-)-pinoresinol has been accomplished by application of the oxidative coupling reaction of benzoylacetate with potassium persulfate as a key step.
Synthesis and N.m.r. Spectra of 2,6- and 2,4-Diaryl-3,7-dioxabicyclooctanes
Pelter, Andrew,Ward, Robert S.,Watson, Derrick J.,Jack, Ibiba R.
, p. 183 - 190 (2007/10/02)
A series of isomeric 2,6- and 2,4-diaryl-3,7-dioxabicyclooctanes have been prepared via the corresponding threo, and erythro-dioxo-diesters.Comparison of their 1H and 13C n.m.r. spectra reveals small differences in chemical shifts and coupling constants which could be diagnostic in assigning structures to such compounds.The structure of 4-hydroxysesamin has been confirmed by direct correlation with sesamin.
