679-85-6Relevant articles and documents
Method and device for preparing 2,3,3,3-tetrafluoropropene
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Paragraph 0084; 0088-0090; 0094; 0098-0100, (2019/01/14)
The invention provides a method and a device for preparing 2,3,3,3-tetrafluoropropene. The device for preparing 2,3,3,3-tetrafluoropropene comprises a circulation flow reactor, a first rectifying tower, a first cooling tower, a second rectifying tower and a second cooling tower. The method provided by the invention adopts a continuous loop reactor technology to realize the technology of separatinghydrogen chloride by-products in real time under the reaction conditions, so that the selectivity of the reaction is greatly improved; since the continuous circulation operation of the raw materialsis realized, the total conversion rate of the reaction is very high. 2,3,3,3-tetrafluoropropene obtained by the method is low in cost; the production technology has the advantages of being few in by-products and wastes and suitable for industrial large-scale production.
REACTIONS OF PENTAKIS(αH,αH,ωH-POLYFLUOROALKOXY)PHOSPHORANES WITH ARENETHIOLS. TETRAKIS(αH,αH,ωH-POLYFLUOROALKOXY)(PHENYLTHIO)PHOSPHORANES
Shermolovich, Yu. G.,Kolesnik, N. P.,Vasil'ev, V. V.,Pashinnik, V. E.,Markovskii, L. N.
, p. 423 - 428 (2007/10/02)
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